diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite borane

Base Information

Chemical Name:diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite borane
CAS No.:1337878-58-6
Molecular Formula:C₁₇H₃₂BO₆P
Molecular Weight:374.222
Hs Code.:

Synonyms:diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite borane

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Chemical Property of diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite borane

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Technology Process of diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite borane

There total 1 articles about diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1337529-87-9
diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite

: 1337878-58-6
diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite borane

Guidance literature:: With dimethylsulfide borane complex; In diethyl ether; hexane; at 20 ℃; for 15h;
DOI:10.1021/ol2020175

Reference yield: 56.0%

: 1337878-58-6
diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite borane

: 1337529-87-9
diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In benzene; at 50 ℃; for 22h;
DOI:10.1021/ol2020175

Reference yield:

: 1337878-58-6
diethyl-3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenylphosphonite borane

: 1337529-97-1
C₆₀H₈₈N₁₁O₁₈P

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-diaza-bicyclo[2.2.2]octane / benzene / 22 h / 50 °C

2: dimethyl sulfoxide / 4 h / 20 °C / pH 8.2 / tris/HCl buffer

With 1,4-diaza-bicyclo[2.2.2]octane; In dimethyl sulfoxide; benzene; 2: Staudinger reaction;
DOI:10.1021/ol2020175