2-azido-3,6-di-O-benzyl-4-O-dibenzylphosphate-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

Base Information

Chemical Name:2-azido-3,6-di-O-benzyl-4-O-dibenzylphosphate-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol
CAS No.:371966-08-4
Molecular Formula:C₆₁H₆₄N₃O₁₃P
Molecular Weight:1078.17
Hs Code.:

Synonyms:2-azido-3,6-di-O-benzyl-4-O-dibenzylphosphate-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

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Chemical Property of 2-azido-3,6-di-O-benzyl-4-O-dibenzylphosphate-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

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Technology Process of 2-azido-3,6-di-O-benzyl-4-O-dibenzylphosphate-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

There total 14 articles about 2-azido-3,6-di-O-benzyl-4-O-dibenzylphosphate-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2-azido-2-deoxy-3,6-di-O-benzyl-4-O-dibenzylphosphate-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-1,2-O-(L-1,7,7-trimethyl-[2.2.1]-bicyclohept-2-yliden)-D-myo-inositol

: 371966-08-4
2-azido-3,6-di-O-benzyl-4-O-dibenzylphosphate-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 2h;
DOI:10.1039/b418041k

Reference yield:

: C₃₆H₄₅N₃O₁₀

: 371966-08-4
2-azido-3,6-di-O-benzyl-4-O-dibenzylphosphate-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

Guidance literature:: Multi-step reaction with 5 steps

1: 1.34 g / NaH / dimethylformamide / 10 h

2: 90 percent / NaCNBH₃; 3 Angstroem molecular sieves; HCl / tetrahydrofuran; diethyl ether / 0.08 h

3: 1H-tetrazole / CH₂Cl₂ / 0.5 h

4: 242 mg / MCPBA / CH₂Cl₂ / 0.17 h / 0 °C

5: 83 percent / aq. TFA / CH₂Cl₂ / 2 h

With 1H-tetrazole; hydrogenchloride; 3 A molecular sieve; sodium hydride; sodium cyanoborohydride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b418041k

Reference yield:

: C₇₁H₇₈N₃O₁₂P

: 371966-08-4
2-azido-3,6-di-O-benzyl-4-O-dibenzylphosphate-2-deoxy-α-D-glucopyranosyl-(1->6)-3,4,5-tri-O-benzyl-D-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 242 mg / MCPBA / CH₂Cl₂ / 0.17 h / 0 °C

2: 83 percent / aq. TFA / CH₂Cl₂ / 2 h

With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/b418041k