phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-3,6-di-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-3,6-di-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside
CAS No.:1439814-61-5
Molecular Formula:C₃₈H₄₈Cl₃NO₂₁S
Molecular Weight:993.218
Hs Code.:

phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-3,6-di-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside

Synonyms:phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-3,6-di-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-3,6-di-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-3,6-di-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside

There total 3 articles about phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-3,6-di-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: C₂₀H₃₂O₅SSn

: C₂₆H₃₃BrCl₃NO₁₆

: 1439814-61-5
phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-3,6-di-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; In dichloromethane; at -40 - 10 ℃; for 6h; regioselective reaction; Inert atmosphere; Molecular sieve; Darkness;
DOI:10.1002/ejoc.201300026

Reference yield:

: 2936-70-1,5624-48-6,13992-15-9,16758-34-2,28244-97-5,77481-62-0,77481-63-1,105088-17-3,149495-84-1
(2R,3S,4S,5R,6S)-2-Hydroxymethyl-6-phenylsulfanyl-tetrahydro-pyran-3,4,5-triol

: 1439814-61-5
phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-3,6-di-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 3 h / Reflux; Inert atmosphere

2: silver trifluoromethanesulfonate / dichloromethane / 6 h / -40 - 10 °C / Inert atmosphere; Molecular sieve; Darkness

With silver trifluoromethanesulfonate; In methanol; dichloromethane;
DOI:10.1002/ejoc.201300026

Reference yield:

: 1329426-52-9
phenyl 1-thio-N-trichloroacetyllactosamine hexaacetate

: 1439814-61-5
phenyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1→4)-3,6-di-O-acetyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1→6)-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / dichloromethane / 20 °C / Inert atmosphere

2: silver trifluoromethanesulfonate / dichloromethane / 6 h / -40 - 10 °C / Inert atmosphere; Molecular sieve; Darkness

With bromine; silver trifluoromethanesulfonate; In dichloromethane;
DOI:10.1002/ejoc.201300026