(S)-tri-tert-butyl 11-((1-(2-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-2-oxo-ethyl)-1H-1,2,3-triazol-4-yl)-methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

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Chemical Name:(S)-tri-tert-butyl 11-((1-(2-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-2-oxo-ethyl)-1H-1,2,3-triazol-4-yl)-methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate
CAS No.:1351304-97-6
Molecular Formula:C₄₀H₆₄N₈O₉
Molecular Weight:800.996
Hs Code.:

(S)-tri-tert-butyl 11-((1-(2-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-2-oxo-ethyl)-1H-1,2,3-triazol-4-yl)-methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

Synonyms:(S)-tri-tert-butyl 11-((1-(2-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-2-oxo-ethyl)-1H-1,2,3-triazol-4-yl)-methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

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Chemical Property of (S)-tri-tert-butyl 11-((1-(2-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-2-oxo-ethyl)-1H-1,2,3-triazol-4-yl)-methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

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Technology Process of (S)-tri-tert-butyl 11-((1-(2-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-2-oxo-ethyl)-1H-1,2,3-triazol-4-yl)-methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

There total 1 articles about (S)-tri-tert-butyl 11-((1-(2-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-2-oxo-ethyl)-1H-1,2,3-triazol-4-yl)-methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 57294-89-0
(3S)-(2-azido-acetylamino)-3-phenyl-propionic acid methyl ester

: 1093239-07-6
11-prop-2-ynyl-1,4,8,11-tetraaza-cyclotetradecane-1,4,8-tricarboxylic acid tri-tert-butyl ester

: 1351304-97-6
(S)-tri-tert-butyl 11-((1-(2-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-2-oxo-ethyl)-1H-1,2,3-triazol-4-yl)-methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 12h;
DOI:10.1021/ic2020012

Reference yield:

: 1351304-97-6
(S)-tri-tert-butyl 11-((1-(2-((1-methoxy-1-oxo-3-phenylpropan-2-yl)amino)-2-oxo-ethyl)-1H-1,2,3-triazol-4-yl)-methyl)-1,4,8,11-tetraazacyclotetradecane-1,4,8-tricarboxylate

: (S)-methyl 2-(2-(4-((1,4,8,11-tetraazacyclotetradecan-1-yl)-methyl)-1H-1,2,3-triazol-1-yl)-acetamido)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane; water / 6 h / 20 °C

2: sodium carbonate / water / pH 11 - 12

With sodium carbonate; In dichloromethane; water;
DOI:10.1021/ic2020012