7-(2',3'-di-O-benzoyl-6'-bromo-6'-desoxy-β-D-glucopyranosyl) theophylline

Base Information

Chemical Name:7-(2',3'-di-O-benzoyl-6'-bromo-6'-desoxy-β-D-glucopyranosyl) theophylline
CAS No.:76139-01-0
Molecular Formula:C₂₇H₂₅BrN₄O₈
Molecular Weight:613.421
Hs Code.:

Synonyms:7-(2',3'-di-O-benzoyl-6'-bromo-6'-desoxy-β-D-glucopyranosyl) theophylline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(2',3'-di-O-benzoyl-6'-bromo-6'-desoxy-β-D-glucopyranosyl) theophylline

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Technology Process of 7-(2',3'-di-O-benzoyl-6'-bromo-6'-desoxy-β-D-glucopyranosyl) theophylline

There total 2 articles about 7-(2',3'-di-O-benzoyl-6'-bromo-6'-desoxy-β-D-glucopyranosyl) theophylline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 76138-97-1
7-(2',3'-di-O-benzoyl-β-D-glucopyranosyl) theophylline

: 76139-01-0
7-(2',3'-di-O-benzoyl-6'-bromo-6'-desoxy-β-D-glucopyranosyl) theophylline

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In N,N-dimethyl-formamide; at 50 ℃; for 3h;

Reference yield:

: 76158-34-4
C₃₄H₃₀N₄O₉

: 76139-01-0
7-(2',3'-di-O-benzoyl-6'-bromo-6'-desoxy-β-D-glucopyranosyl) theophylline

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / aq. acetic acid / 1 h / 100 °C

2: 72 percent / N-bromosuccinimide, triphenylphosphine / dimethylformamide / 3 h / 50 °C

With N-Bromosuccinimide; triphenylphosphine; In acetic acid; N,N-dimethyl-formamide;