4-(5-chlorobenzothiazol-2-yl)-2,6-difluorophenyl dihydrogen phosphate

Base Information

Chemical Name:4-(5-chlorobenzothiazol-2-yl)-2,6-difluorophenyl dihydrogen phosphate
CAS No.:1564104-06-8
Molecular Formula:C₁₃H₇ClF₂NO₄PS
Molecular Weight:377.692
Hs Code.:

Synonyms:4-(5-chlorobenzothiazol-2-yl)-2,6-difluorophenyl dihydrogen phosphate

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Chemical Property of 4-(5-chlorobenzothiazol-2-yl)-2,6-difluorophenyl dihydrogen phosphate

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Technology Process of 4-(5-chlorobenzothiazol-2-yl)-2,6-difluorophenyl dihydrogen phosphate

There total 6 articles about 4-(5-chlorobenzothiazol-2-yl)-2,6-difluorophenyl dihydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1564102-71-1
4-(5-chlorobenzothiazol-2-yl)-2,6-difluorophenyl dibenzyl phosphate

: 1564104-06-8
4-(5-chlorobenzothiazol-2-yl)-2,6-difluorophenyl dihydrogen phosphate

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 24h;
DOI:10.1016/j.bmc.2014.01.013

Reference yield:

: 654-11-5
3,5-Difluoro-4-methoxybenzaldehyde

: 1564104-06-8
4-(5-chlorobenzothiazol-2-yl)-2,6-difluorophenyl dihydrogen phosphate

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethanol / 18 h / 20 °C

2.1: chloranil / dichloromethane / 20 h / 20 °C

3.1: Pyridine hydrobromide / 1.5 h / Inert atmosphere; Heating

4.1: tetrachloromethane; N-ethyl-N,N-diisopropylamine; dmap / acetonitrile / 0.02 h / -10 °C

4.2: 1.5 h / -10 °C

5.1: trifluoroacetic acid / 24 h / 20 °C

With tetrachloromethane; dmap; Pyridine hydrobromide; chloranil; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In ethanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2014.01.013

Reference yield:

: 1564086-99-2
C₁₄H₁₀ClF₂NOS

: 1564104-06-8
4-(5-chlorobenzothiazol-2-yl)-2,6-difluorophenyl dihydrogen phosphate

Guidance literature:: Multi-step reaction with 4 steps

1.1: chloranil / dichloromethane / 20 h / 20 °C

2.1: Pyridine hydrobromide / 1.5 h / Inert atmosphere; Heating

3.1: tetrachloromethane; N-ethyl-N,N-diisopropylamine; dmap / acetonitrile / 0.02 h / -10 °C

3.2: 1.5 h / -10 °C

4.1: trifluoroacetic acid / 24 h / 20 °C

With tetrachloromethane; dmap; Pyridine hydrobromide; chloranil; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2014.01.013