carbonylnitrosyl{1-(pentacarbonylchromium)-2-(2,4,6-tri-tert-butylphenyl)diphosphenyl}(pentamethylcyclopentadienyl)rhenium

Base Information

Chemical Name:carbonylnitrosyl{1-(pentacarbonylchromium)-2-(2,4,6-tri-tert-butylphenyl)diphosphenyl}(pentamethylcyclopentadienyl)rhenium
CAS No.:111960-41-9
Molecular Formula:C₃₄H₄₄CrNO₇P₂Re
Molecular Weight:878.876
Hs Code.:

Synonyms:carbonylnitrosyl{1-(pentacarbonylchromium)-2-(2,4,6-tri-tert-butylphenyl)diphosphenyl}(pentamethylcyclopentadienyl)rhenium

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Chemical Property of carbonylnitrosyl{1-(pentacarbonylchromium)-2-(2,4,6-tri-tert-butylphenyl)diphosphenyl}(pentamethylcyclopentadienyl)rhenium

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Technology Process of carbonylnitrosyl{1-(pentacarbonylchromium)-2-(2,4,6-tri-tert-butylphenyl)diphosphenyl}(pentamethylcyclopentadienyl)rhenium

There total 1 articles about carbonylnitrosyl{1-(pentacarbonylchromium)-2-(2,4,6-tri-tert-butylphenyl)diphosphenyl}(pentamethylcyclopentadienyl)rhenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 92937-36-5,92889-73-1
pentacarbonyl(η2-cis-cyclooctene)chromium(0)

: 111960-39-5
(η5-C5(CH3)5)(CO)(NO)RePP(2,4,6-tBu3C6H2)

: 931-88-4,931-87-3,25267-51-0
cis-Cyclooctene

: 111960-41-9
carbonylnitrosyl{1-(pentacarbonylchromium)-2-(2,4,6-tri-tert-butylphenyl)diphosphenyl}(pentamethylcyclopentadienyl)rhenium

Guidance literature:: In tetrahydrofuran; hexane; under N2, addn. of soln. of ((Z)-C8H14)Cr(CO)5 in hexane to a freshly prepd. soln. of Re-compound in THF at 0°C, stirred 1 h at 20°C; evapn. to dryness, dissolved in ether, filtration, concn. of filtrate, crystn. at -28°C for 12 h; elem. anal.;