3-N-(3-chlorophenyl)-4,5-tetramethylene thieno-[2,3-d][1,2,3]-triazin-4(3H)-one

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Chemical Name:3-N-(3-chlorophenyl)-4,5-tetramethylene thieno-[2,3-d][1,2,3]-triazin-4(3H)-one
CAS No.:1246527-92-3
Molecular Formula:C₁₅H₁₂ClN₃OS
Molecular Weight:317.799
Hs Code.:

Synonyms:3-N-(3-chlorophenyl)-4,5-tetramethylene thieno-[2,3-d][1,2,3]-triazin-4(3H)-one

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Chemical Property of 3-N-(3-chlorophenyl)-4,5-tetramethylene thieno-[2,3-d][1,2,3]-triazin-4(3H)-one

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Technology Process of 3-N-(3-chlorophenyl)-4,5-tetramethylene thieno-[2,3-d][1,2,3]-triazin-4(3H)-one

There total 2 articles about 3-N-(3-chlorophenyl)-4,5-tetramethylene thieno-[2,3-d][1,2,3]-triazin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 63503-60-6
3-chlorophenylboronic acid

: 38359-86-3
4,5-tetramethylene thieno-[2,3-d][1,2,3]-triazin-4(3H)-one

: 1246527-92-3
3-N-(3-chlorophenyl)-4,5-tetramethylene thieno-[2,3-d][1,2,3]-triazin-4(3H)-one

Guidance literature:: With copper diacetate; triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 1.5h;
DOI:10.1016/j.bmcl.2011.11.096

Reference yield: 71.0%

: 85930-58-1
2-Amino-4,5,6,7-tetrahydro-benzo[b]thiophene-3-carboxylic acid (3-chloro-phenyl)-amide

: 1246527-92-3
3-N-(3-chlorophenyl)-4,5-tetramethylene thieno-[2,3-d][1,2,3]-triazin-4(3H)-one

Guidance literature:: 2-Amino-4,5,6,7-tetrahydro-benzo[b]thiophene-3-carboxylic acid (3-chloro-phenyl)-amide; With hydrogenchloride; In water; acetic acid; at 5 - 20 ℃;

With sodium nitrite; In water; acetic acid; at 0 - 5 ℃;
DOI:10.1016/j.ejmech.2010.05.061