9,20-bis[2-(octoxy)benzoyl]-7,18-dihydrodinaphtho[b,i][1,4,8,11]tetraazacyclotetradecine

Base Information

Chemical Name:9,20-bis[2-(octoxy)benzoyl]-7,18-dihydrodinaphtho[b,i][1,4,8,11]tetraazacyclotetradecine
CAS No.:1446680-86-9
Molecular Formula:C₅₆H₆₀N₄O₄
Molecular Weight:853.117
Hs Code.:

Synonyms:9,20-bis[2-(octoxy)benzoyl]-7,18-dihydrodinaphtho[b,i][1,4,8,11]tetraazacyclotetradecine

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Chemical Property of 9,20-bis[2-(octoxy)benzoyl]-7,18-dihydrodinaphtho[b,i][1,4,8,11]tetraazacyclotetradecine

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Technology Process of 9,20-bis[2-(octoxy)benzoyl]-7,18-dihydrodinaphtho[b,i][1,4,8,11]tetraazacyclotetradecine

There total 2 articles about 9,20-bis[2-(octoxy)benzoyl]-7,18-dihydrodinaphtho[b,i][1,4,8,11]tetraazacyclotetradecine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 111-83-1
1-bromo-octane

: 1446680-85-8
9,20-bis(2-hydroxybenzoyl)-7,18-dihydrodinaphtho[b,i][1,4,8,11]tetraazacyclotetradecine

: 1446680-86-9
9,20-bis[2-(octoxy)benzoyl]-7,18-dihydrodinaphtho[b,i][1,4,8,11]tetraazacyclotetradecine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 5h;
DOI:10.1080/10610278.2013.766736

Reference yield:

: 771-97-1
2,3-Diaminonaphthalene

: 1446680-86-9
9,20-bis[2-(octoxy)benzoyl]-7,18-dihydrodinaphtho[b,i][1,4,8,11]tetraazacyclotetradecine

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform / 1 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 5 h / 80 °C

With potassium carbonate; In chloroform; N,N-dimethyl-formamide;
DOI:10.1080/10610278.2013.766736