(5,15-bis(3-hydroxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc

Base Information

• Chemical Name: (5,15-bis(3-hydroxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc
• CAS No.: 795281-76-4
• Molecular Formula: C₅₂H₆₀N₄O₂Zn
• Molecular Weight: 838.464

Synonyms:(5,15-bis(3-hydroxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc

Chemical Property of (5,15-bis(3-hydroxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc

Chemical Property:

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Technology Process of (5,15-bis(3-hydroxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc

There total 1 articles about (5,15-bis(3-hydroxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(5,15-bis(3-methoxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc (158595-88-1) → (5,15-bis(3-hydroxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc (795281-76-4)

Guidance literature:

With methanol; boron tribromide; In chloroform; a soln. of BBr3 added to a soln. of Zn complex, stirred, MeOH added, stirred; neutralized with NH3 soln., evapd., chromd. (silica gel, CHCl3);

DOI:10.1007/s11176-005-0029-0

Reference yield:

L-Alanine methyl ester (10065-72-2) + (5,15-bis(3-hydroxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc (795281-76-4) → [2,8,12,18-tetrabutyl-5,15-bis(3-hydroxyphenyl)-3,7,13,17-tetramethylporphyrinato]zinc L-α-alanine methyl ester

Guidance literature:

In toluene; spectrophotometric titration at 20°C; not isolated;

DOI:10.1007/s11176-005-0029-0

Reference yield:

(5,15-bis(3-hydroxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc (795281-76-4) + methoxycarbonylmethylamine (616-34-2) → [2,8,12,18-tetrabutyl-5,15-bis(3-hydroxyphenyl)-3,7,13,17-tetramethylporphyrinato]zinc glycine methyl ester

Guidance literature:

In toluene; spectrophotometric titration at 20°C; not isolated;

DOI:10.1007/s11176-005-0029-0

upstream raw materials:

(5,15-bis(3-methoxyphenyl)-2,8,12,18-tetra-n-butyl-3,7,13,17-tetramethylporphyrinato)zinc

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