C₃₆H₅₀O₇Si

Base Information

Chemical Name:C₃₆H₅₀O₇Si
CAS No.:1032880-17-3
Molecular Formula:C₃₆H₅₀O₇Si
Molecular Weight:622.874
Hs Code.:

C<sub>36</sub>H<sub>50</sub>O<sub>7</sub>Si

Synonyms:C₃₆H₅₀O₇Si

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Chemical Property of C₃₆H₅₀O₇Si

Chemical Property:

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Technology Process of C₃₆H₅₀O₇Si

There total 14 articles about C₃₆H₅₀O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1032880-15-1
C₃₆H₅₂O₇Si

: 1032880-17-3
C₃₆H₅₀O₇Si

Guidance literature:: C₃₆H₅₂O₇Si; With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In dichloromethane; at 0 ℃; for 2h;

Molecular sieve;
DOI:10.1021/ol8008057

Reference yield:

: 101331-92-4
4-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-L-threose

: 1032880-17-3
C₃₆H₅₀O₇Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: (-)-B-methoxydiisopinocamphenylborane / diethyl ether / 1 h / 0 - 20 °C

1.2: 3 h / -78 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / -10 - 20 °C

2.2: 12 h / 20 °C

3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C

3.2: 2 h / Reflux

4.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

5.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 1 h / -10 - 20 °C

6.1: toluene-4-sulfonic acid / dichloromethane / 3 h / 0 - 20 °C

7.1: pyridine; dmap / dichloromethane / 20 °C

8.1: tetrahydrofuran / 1 h / -78 °C

8.2: 0.03 h / -78 °C / Molecular sieve

9.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 8 h / 20 °C

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.5 h / 20 °C

11.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / 0 °C

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; (-)-B-methoxydiisopinocamphenylborane; sulfur trioxide pyridine complex; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.3987/COM-12-S(N)54

Reference yield:

: 1032879-81-4
C₂₇H₃₈O₄Si

: 1032880-17-3
C₃₆H₅₀O₇Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 5 h / 0 - 20 °C

1.2: 2 h / Reflux

2.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / -10 °C

3.1: 2-methyl-but-2-ene; sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 1 h / -10 - 20 °C

4.1: toluene-4-sulfonic acid / dichloromethane / 3 h / 0 - 20 °C

5.1: pyridine; dmap / dichloromethane / 20 °C

6.1: tetrahydrofuran / 1 h / -78 °C

6.2: 0.03 h / -78 °C / Molecular sieve

7.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 8 h / 20 °C

8.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.5 h / 20 °C

9.1: dimethyl sulfoxide; triethylamine; sulfur trioxide pyridine complex / dichloromethane / 2 h / 0 °C

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; sulfur trioxide pyridine complex; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.3987/COM-12-S(N)54