benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-(dibenzylphosphoryl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate

Base Information

• Chemical Name: benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-(dibenzylphosphoryl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate
• CAS No.: 875066-24-3
• Molecular Formula: C₄₀H₄₆NO₁₆P
• Molecular Weight: 827.776

Synonyms:benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-(dibenzylphosphoryl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate

Chemical Property of benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-(dibenzylphosphoryl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-(dibenzylphosphoryl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate

There total 3 articles about benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-(dibenzylphosphoryl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-O-(dibenzylphosphityl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate → benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-(dibenzylphosphoryl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate (875066-24-3)

Guidance literature:

With tert.-butylhydroperoxide; In acetonitrile; at -20 - 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/chem.201003387

Reference yield:

dibenzyl chlorophosphite (41662-50-4) → benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-(dibenzylphosphoryl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate (875066-24-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1H-tetrazole / acetone / 0.5 h / -20 - 20 °C / Inert atmosphere

2: tert.-butylhydroperoxide / acetonitrile / 0.5 h / -20 - 20 °C / Inert atmosphere

With 1H-tetrazole; tert.-butylhydroperoxide; In acetone; acetonitrile;

DOI:10.1002/chem.201003387

Reference yield:

Benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate → benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-(dibenzylphosphoryl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate (875066-24-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1H-tetrazole / acetone / 0.5 h / -20 - 20 °C / Inert atmosphere

2: tert.-butylhydroperoxide / acetonitrile / 0.5 h / -20 - 20 °C / Inert atmosphere

With 1H-tetrazole; tert.-butylhydroperoxide; In acetone; acetonitrile;

DOI:10.1002/chem.201003387

upstream raw materials:

dibenzyl chlorophosphite

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 875066-24-3 benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2-(dibenzylphosphoryl)-3,5-dideoxy-β-D-glycero-D-galacto-2-nonulopyranosonate

Send

Send

Metric Ton KG G Pound L ML

Send

Send