methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoate

Base Information

• Chemical Name: methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoate
• CAS No.: 1620775-45-2
• Molecular Formula: C₁₃H₁₀ClF₃N₄O₃
• Molecular Weight: 364.68

Synonyms:methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoate

Chemical Property of methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoate

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Technology Process of methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoate

There total 1 articles about methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C5(2)H2Cl2F3N3O (1620775-44-1) + 4-methoxycarbonyl aniline (619-45-4) → methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D2)-1,3,5-triazin-2-ylamino)benzoate (1620775-45-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; at 20 ℃; for 16h;

Reference yield:

methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D2)-1,3,5-triazin-2-ylamino)benzoate (1620775-45-2) + 1-(4-chlorophenyl)cyclopropane-1-amine (72934-36-2) → methyl 4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D2)-1,3,5-triazin-2-ylamino)benzoate (1620775-46-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 70 ℃; for 16h;

Reference yield:

methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D2)-1,3,5-triazin-2-ylamino)benzoate (1620775-45-2) → 4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D2)-1,3,5-triazin-2-ylamino)benzoic acid (1620775-42-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 70 °C

2.1: potassium carbonate / acetone; water / 16 h / 80 °C / Sealed tube

2.2: pH 2

With potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; acetone;

upstream raw materials:

C₅⁽²⁾H₂Cl₂F₃N₃O

4-methoxycarbonyl aniline

Downstream raw materials:

4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoic acid

4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoyl chloride

2-(4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzamido)-N,N,N-trimethylethanaminium

methyl 4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoate

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