C₇₂H₅₄O₉

Base Information

Chemical Name:C₇₂H₅₄O₉
CAS No.:1446146-20-8
Molecular Formula:C₇₂H₅₄O₉
Molecular Weight:1063.22
Hs Code.:

C<sub>72</sub>H<sub>54</sub>O<sub>9</sub>

Synonyms:C₇₂H₅₄O₉

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Chemical Property of C₇₂H₅₄O₉

Chemical Property:

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Technology Process of C₇₂H₅₄O₉

There total 8 articles about C₇₂H₅₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1446146-22-0
C₇₅H₆₀O₉

: 1446146-20-8
C₇₂H₅₄O₉

Guidance literature:: With water; hydrogen bromide; In acetic acid; at 130 ℃; for 17h;
DOI:10.1039/c3cc43358g

Reference yield:

: 1446146-19-5
C₇₅H₆₆O₉

: 1446146-20-8
C₇₂H₅₄O₉

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

2: hydrogen bromide; water / acetic acid / 17 h / 130 °C

With water; hydrogen bromide; pyridinium chlorochromate; In dichloromethane; acetic acid;
DOI:10.1039/c3cc43358g

Reference yield:

: 3-iodo-[1,1'-biphenyl]-2-carboxylic acid

: 1446146-20-8
C₇₂H₅₄O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / tetrahydrofuran; water / 7 h / 50 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: 1 h / -78 - 20 °C / Inert atmosphere

4.1: pyridinium chlorochromate / dichloromethane / 2 h / 20 °C

5.1: hydrogen bromide; water / acetic acid / 17 h / 130 °C

With bis-triphenylphosphine-palladium(II) chloride; n-butyllithium; water; hydrogen bromide; sodium carbonate; caesium carbonate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c3cc43358g