6-(Benzyloxycarbonylamino)-6-deoxy-1,2:3,4-di-O-isopropylidene-6-(2-thiazolyl)-β-L-glycero-D-galacto-1,5-hexopyranoside

Base Information

Chemical Name:6-(Benzyloxycarbonylamino)-6-deoxy-1,2:3,4-di-O-isopropylidene-6-(2-thiazolyl)-β-L-glycero-D-galacto-1,5-hexopyranoside
CAS No.:147455-52-5
Molecular Formula:C₂₃H₂₈N₂O₇S
Molecular Weight:476.551
Hs Code.:

Synonyms:6-(Benzyloxycarbonylamino)-6-deoxy-1,2:3,4-di-O-isopropylidene-6-(2-thiazolyl)-β-L-glycero-D-galacto-1,5-hexopyranoside

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Chemical Property of 6-(Benzyloxycarbonylamino)-6-deoxy-1,2:3,4-di-O-isopropylidene-6-(2-thiazolyl)-β-L-glycero-D-galacto-1,5-hexopyranoside

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Technology Process of 6-(Benzyloxycarbonylamino)-6-deoxy-1,2:3,4-di-O-isopropylidene-6-(2-thiazolyl)-β-L-glycero-D-galacto-1,5-hexopyranoside

There total 3 articles about 6-(Benzyloxycarbonylamino)-6-deoxy-1,2:3,4-di-O-isopropylidene-6-(2-thiazolyl)-β-L-glycero-D-galacto-1,5-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 147455-51-4
C-[(R)-C-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-Tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-C-thiazol-2-yl]-methylamine

: 147455-52-5
6-(Benzyloxycarbonylamino)-6-deoxy-1,2:3,4-di-O-isopropylidene-6-(2-thiazolyl)-β-L-glycero-D-galacto-1,5-hexopyranoside

Guidance literature:: With sodium hydrogencarbonate; In 1,4-dioxane; at 0 ℃; for 0.333333h; Yield given;

Reference yield:

: 191997-37-2,147455-48-9
(Z)-N-benzyl-(1,2:3,4-di-O-isopropylidene-α-D-galactopyranos-6-ylidene)amine N-oxide

: 147455-52-5
6-(Benzyloxycarbonylamino)-6-deoxy-1,2:3,4-di-O-isopropylidene-6-(2-thiazolyl)-β-L-glycero-D-galacto-1,5-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / ZnBr₂ / diethyl ether; hexane / 1.) -78 deg C, 15 min, 2.) -80 deg C, 30 min

2: 20percent aq. TiCl₃ / methanol / 0.25 h / Ambient temperature

3: 7percent aq. NaHCO₃ / dioxane / 0.33 h / 0 °C

With titanium(III) chloride; sodium hydrogencarbonate; zinc dibromide; In 1,4-dioxane; methanol; diethyl ether; hexane;

Reference yield:

: 147455-49-0
N-Benzyl-6-deoxy-6-(hydroxyamino)-1,2:3,4-O-isopropylidene-6-(2-thiazolyl)-β-L-glycero-D-galacto-1,5-hexopyranoside

: 147455-52-5
6-(Benzyloxycarbonylamino)-6-deoxy-1,2:3,4-di-O-isopropylidene-6-(2-thiazolyl)-β-L-glycero-D-galacto-1,5-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 20percent aq. TiCl₃ / methanol / 0.25 h / Ambient temperature

2: 7percent aq. NaHCO₃ / dioxane / 0.33 h / 0 °C

With titanium(III) chloride; sodium hydrogencarbonate; In 1,4-dioxane; methanol;