(S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid

Base Information

• Chemical Name: (S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid
• CAS No.: 713122-72-6
• Molecular Formula: C₂₄H₃₂O₄Si
• Molecular Weight: 412.601

Synonyms:(S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid

Chemical Property of (S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid

Chemical Property:

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Technology Process of (S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid

There total 2 articles about (S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

(S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester (713122-71-5) → (S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid (713122-72-6)

Guidance literature:

With potassium trimethylsilonate; In diethyl ether; at 20 ℃;

DOI:10.1021/ol049483s

Reference yield:

(S)-methyl 4-(tert-butyldiphenylsilyloxy)-3-hydroxybutanoate (124655-05-6) → (S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid (713122-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / CF₃SO₃H / CH₂Cl₂ / 20 °C

2: 86 percent / potassium trimethylsilanolate / diethyl ether / 20 °C

With trifluorormethanesulfonic acid; potassium trimethylsilonate; In diethyl ether; dichloromethane;

DOI:10.1021/ol049483s

Reference yield:

(S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid (713122-72-6) → (S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyryl chloride

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃;

DOI:10.1021/ol049483s

upstream raw materials:

(S)-3-[((E)-But-2-enyl)oxy]-4-(tert-butyl-diphenyl-silanyloxy)-butyric acid methyl ester

(S)-methyl 4-(tert-butyldiphenylsilyloxy)-3-hydroxybutanoate

Downstream raw materials:

(2R,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-2-((S)-1-methyl-allyl)-dihydro-furan-3-one

(S)-4-[((E)-But-2-enyl)oxy]-5-(tert-butyl-diphenyl-silanyloxy)-1-diazo-pentan-2-one

(S)-3-[(2R,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-oxo-tetrahydro-furan-2-yl]-butyric acid

(S)-3-[(2R,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-oxo-tetrahydro-furan-2-yl]-butyric acid methyl ester

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