C₆₂H₆₈O₂Si

Base Information

Chemical Name:C₆₂H₆₈O₂Si
CAS No.:775306-58-6
Molecular Formula:C₆₂H₆₈O₂Si
Molecular Weight:873.306
Hs Code.:

C<sub>62</sub>H<sub>68</sub>O<sub>2</sub>Si

Synonyms:C₆₂H₆₈O₂Si

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Chemical Property of C₆₂H₆₈O₂Si

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Technology Process of C₆₂H₆₈O₂Si

There total 3 articles about C₆₂H₆₈O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 606098-82-2
1,4-bis(hexyloxy)-2-ethynyl-5-(2-triisopropylsilylethynyl)benzene

: 775306-56-4
C₃₂H₁₉F₃O₃S

: 775306-58-6
C₆₂H₆₈O₂Si

Guidance literature:: With piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 50 ℃; for 8h;
DOI:10.1021/ma048728d

Reference yield:

: 17274-18-9
sodium 2-(4-methoxyphenyl)acetate

: 775306-58-6
C₆₂H₆₈O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1: 37 percent / acetic anhydride / 2 h / 150 °C

2: 42 percent / PdCl₂(PPh₃)2; 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-acetamide / 12 h / 160 °C

3: 96 percent / BBr₃ / CH₂Cl₂ / -78 - 20 °C

4: 68 percent / pyridine / 0 - 20 °C

5: 68 percent / Pd(PPh₃)4; CuI; piperidine / tetrahydrofuran / 8 h / 50 °C

With piperidine; pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic anhydride; boron tribromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide;
DOI:10.1021/ma048728d

Reference yield:

: C₂₄H₁₇Br₂O⁽¹⁺⁾*BF₄^(1-)

: 775306-58-6
C₆₂H₆₈O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1: 37 percent / acetic anhydride / 2 h / 150 °C

2: 42 percent / PdCl₂(PPh₃)2; 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-acetamide / 12 h / 160 °C

3: 96 percent / BBr₃ / CH₂Cl₂ / -78 - 20 °C

4: 68 percent / pyridine / 0 - 20 °C

5: 68 percent / Pd(PPh₃)4; CuI; piperidine / tetrahydrofuran / 8 h / 50 °C

With piperidine; pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic anhydride; boron tribromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide;
DOI:10.1021/ma048728d