4-dimethylsulfylimino-3-phenylfuroxan

Base Information

• Chemical Name: 4-dimethylsulfylimino-3-phenylfuroxan
• CAS No.: 130319-35-6
• Molecular Formula: C₁₀H₁₁N₃O₂S
• Molecular Weight: 237.282
• Mol file: 130319-35-6.mol

Synonyms:4-dimethylsulfylimino-3-phenylfuroxan

Chemical Property of 4-dimethylsulfylimino-3-phenylfuroxan

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-dimethylsulfylimino-3-phenylfuroxan

There total 2 articles about 4-dimethylsulfylimino-3-phenylfuroxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-amino-3-phenylfuroxane (30059-86-0) + dimethyl(trifluoromethanesulfonyloxy)sulfonium trifluoromethanesulfonate (55153-71-4) → 4-dimethylsulfylimino-3-phenylfuroxan (130319-35-6)

Guidance literature:

In dichloromethane; dimethyl sulfoxide; at -60 ℃; for 0.5h; Yield given;

DOI:10.1007/BF00957864

Reference yield:

4-amino-3-phenylfuroxane (30059-86-0) + S,S-dimethyl-S-(trifluoroacetoxy)sulfonium trifluoroacetate (57738-66-6) → 4-dimethylsulfylimino-3-phenylfuroxan (130319-35-6)

Guidance literature:

In dichloromethane; dimethyl sulfoxide; at -60 ℃; for 2.5h; Yield given;

DOI:10.1007/BF00957864

Reference yield: 93.0%

4-dimethylsulfylimino-3-phenylfuroxan (130319-35-6) → 4-nitroso-3-phenylfuroxan (130319-33-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -5 ℃; for 0.5h;

DOI:10.1007/BF00957864

upstream raw materials:

4-amino-3-phenylfuroxane

dimethyl(trifluoromethanesulfonyloxy)sulfonium trifluoromethanesulfonate

S,S-dimethyl-S-(trifluoroacetoxy)sulfonium trifluoroacetate

Downstream raw materials:

4-nitroso-3-phenylfuroxan

4-nitro-3-phenylfuroxan

Refernces