C₄₉H₇₂O₈Si₂

Base Information

Chemical Name:C₄₉H₇₂O₈Si₂
CAS No.:1427032-05-0
Molecular Formula:C₄₉H₇₂O₈Si₂
Molecular Weight:845.277
Hs Code.:

C<sub>49</sub>H<sub>72</sub>O<sub>8</sub>Si<sub>2</sub>

Synonyms:C₄₉H₇₂O₈Si₂

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Chemical Property of C₄₉H₇₂O₈Si₂

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Technology Process of C₄₉H₇₂O₈Si₂

There total 22 articles about C₄₉H₇₂O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1427032-04-9
C₅₁H₇₆O₈Si₂

: 1427032-05-0
C₄₉H₇₂O₈Si₂

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; p-benzoquinone; In toluene; at 140 ℃;
DOI:10.1021/ol400408w

Reference yield:

: 1427032-00-5
C₁₉H₂₆O₇

: 1427032-05-0
C₄₉H₇₂O₈Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: chromium dichloride / tetrahydrofuran; N,N-dimethyl-formamide / 4 h / 20 °C

2: lithium hydroxide monohydrate / tetrahydrofuran; water; methanol / 0 - 20 °C

3: triethylamine / tetrahydrofuran / 0.83 h / 0 - 20 °C

4: dmap / toluene / 1.5 h / 20 °C

5: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / toluene / 140 °C

With chromium dichloride; dmap; Hoveyda-Grubbs catalyst second generation; lithium hydroxide monohydrate; triethylamine; p-benzoquinone; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene; 1: |Takai-Utimoto Olefination / 3: |Yamaguchi Lactonization;
DOI:10.1021/ol400408w

Reference yield:

: 1427032-02-7
C₁₉H₂₆O₆

: 1427032-05-0
C₄₉H₇₂O₈Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran / 0.83 h / 0 - 20 °C

2: dmap / toluene / 1.5 h / 20 °C

3: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / toluene / 140 °C

With dmap; Hoveyda-Grubbs catalyst second generation; triethylamine; p-benzoquinone; In tetrahydrofuran; toluene; 1: |Yamaguchi Lactonization;
DOI:10.1021/ol400408w