<(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranoside

Base Information

Chemical Name:<(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranoside
CAS No.:230634-87-4
Molecular Formula:C₄₀H₄₈Cl₂O₁₁S
Molecular Weight:807.787
Hs Code.:

<(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranoside

Synonyms:<(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranoside

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Chemical Property of <(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranoside

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Technology Process of <(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranoside

There total 1 articles about <(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2,6-dichlorophenyl <(2,3,6-trideoxy-4-ulo-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-thio-α-L-galactopyranoside

: 230634-87-4
<(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranoside

Guidance literature:: With 3,3-dimethyldioxirane; sodium hydrogencarbonate; In dichloromethane; acetone; at -72 - -45 ℃;
DOI:10.1021/ja990690a

Reference yield: 75.0%

: 21288-61-9
Epsilon-pyrromycinone

: 230634-87-4
<(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranoside

: 167012-88-6
7-O-<(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranosyl>-ε-pyrromycinone

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; 1,2-dimethoxy-4-(2-propenyl)benzene; In dichloromethane; at -78 ℃; for 0.333333h;
DOI:10.1021/ja990690a

Reference yield:

: 230634-87-4
<(2,3,6-trideoxy-4-ulo-α-L-hexopyranosyl)-(1->4)-<2,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-galactopyranosyl>>-(1->4)-2,6-dideoxy-3-O-(4-methoxybenzyl)-1-(2,6-dichlorophenylsulfinyl)-α-L-galactopyranoside

: 111233-40-0,143396-46-7
ciclamycin 0

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 4-allyl-1,2-dimethoxybenzene, 2,6-di-tert-butyl-4-methylpyridine, triflic anhydride / CH₂Cl₂ / 0.33 h / -78 °C

2: 60 percent / aq. DDQ / CH₂Cl₂ / 0.5 h / Ambient temperature

With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; 1,2-dimethoxy-4-(2-propenyl)benzene; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1021/ja990690a