-N-<(1R)-2-oxocyclopentyl>amino>acetonitrile

Base Information

• Chemical Name: -N-<(1R)-2-oxocyclopentyl>amino>acetonitrile
• CAS No.: 98244-61-2
• Molecular Formula: C₁₅H₁₈N₂O
• Molecular Weight: 242.321

Synonyms:-N-<(1R)-2-oxocyclopentyl>amino>acetonitrile

Chemical Property of -N-<(1R)-2-oxocyclopentyl>amino>acetonitrile

Chemical Property:

Purity/Quality:

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Technology Process of -N-<(1R)-2-oxocyclopentyl>amino>acetonitrile

There total 2 articles about -N-<(1R)-2-oxocyclopentyl>amino>acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

-N-<(R)-α-methylbenzyl>amino>acetonitrile (98237-97-9) → -N-<(1R)-2-oxocyclopentyl>amino>acetonitrile (98244-61-2)

Guidance literature:

With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; for 10h; Ambient temperature;

DOI:10.1002/hlca.19850680324

Reference yield:

(1R,2R)-2-((R)-1-Phenyl-ethylamino)-cyclopentanol; hydrochloride → -N-<(1R)-2-oxocyclopentyl>amino>acetonitrile (98244-61-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / 10 h / Ambient temperature

2: 95 percent / oxalyl chloride, DMSO / CH₂Cl₂ / 10 h / Ambient temperature

With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane;

DOI:10.1002/hlca.19850680324

Reference yield: 91.0%

{1-[3,4-(methylenedioxy)phenyl]vinyl}lithium (79076-14-5) + -N-<(1R)-2-oxocyclopentyl>amino>acetonitrile (98244-61-2) → -N-<(R)-α-methylbenzyl>amino>acetonitrile

Guidance literature:

In tetrahydrofuran; at -75 - -70 ℃; for 1h;

DOI:10.1002/hlca.19850680324

upstream raw materials:

-N-<(R)-α-methylbenzyl>amino>acetonitrile

Downstream raw materials:

(3aS,7aR)-1-<(R)-α-methylbenzyl>-3a-<3,4-(methylenedioxy)phenyl>-2,3,3a,4,5,6,7,7a-octahydro-4(1H)-indolone

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