Technology Process of C10H14N4
There total 4 articles about C10H14N4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(l) iodide; sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; N,N`-dimethylethylenediamine;
In
water; dimethyl sulfoxide;
at 20 ℃;
for 1h;
DOI:10.1002/ejoc.201301838
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium nitrite; sulfuric acid / ethanol / 0 °C / Reflux
2: tin(II) chloride dihdyrate; ethanol / Reflux
3: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C
With
copper(l) iodide; sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; sulfuric acid; N,N`-dimethylethylenediamine; sodium nitrite;
In
ethanol; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201301838
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tin(II) chloride dihdyrate; ethanol / Reflux
2: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C
With
copper(l) iodide; sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; N,N`-dimethylethylenediamine;
In
water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201301838