2-(dicyclohexylphosphanyl)-N-(2-(dicyclohexylphosphanyl)ethyl)-N-methylethan-1-amine

Base Information

Chemical Name:2-(dicyclohexylphosphanyl)-N-(2-(dicyclohexylphosphanyl)ethyl)-N-methylethan-1-amine
CAS No.:1221191-19-0
Molecular Formula:C₂₉H₅₅NP₂
Molecular Weight:479.71
Hs Code.:

Synonyms:2-(dicyclohexylphosphanyl)-N-(2-(dicyclohexylphosphanyl)ethyl)-N-methylethan-1-amine

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Chemical Property of 2-(dicyclohexylphosphanyl)-N-(2-(dicyclohexylphosphanyl)ethyl)-N-methylethan-1-amine

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Technology Process of 2-(dicyclohexylphosphanyl)-N-(2-(dicyclohexylphosphanyl)ethyl)-N-methylethan-1-amine

There total 1 articles about 2-(dicyclohexylphosphanyl)-N-(2-(dicyclohexylphosphanyl)ethyl)-N-methylethan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 55-86-7
mechlorethamine hydrochloride

: 829-84-5
dicyclohexylphosphane

: 1221191-19-0
2-(dicyclohexylphosphanyl)-N-(2-(dicyclohexylphosphanyl)ethyl)-N-methylethan-1-amine

Guidance literature:: dicyclohexylphosphane; With n-butyllithium; In tetrahydrofuran; for 1h; Schlenk technique; Reflux;

mechlorethamine hydrochloride; With n-butyllithium; In tetrahydrofuran; Schlenk technique; Reflux;
DOI:10.1021/jacs.7b05939

Reference yield: 84.0%

: 14516-54-2
bromopentacarbonylmanganese(I)

: 1221191-19-0
2-(dicyclohexylphosphanyl)-N-(2-(dicyclohexylphosphanyl)ethyl)-N-methylethan-1-amine

: C₃₁H₅₅BrMnNO₂P₂

Guidance literature:: In toluene; at 110 ℃; for 20h; Inert atmosphere;
DOI:10.1021/jacs.7b05939

Reference yield: 78.0%

: tetrakis[3,5-bis(trifluoromethyl)phenyl]boric acid bis(diethyl ether) complex

: 1221276-10-3
[Co(CH₂SiMe₃)₂(pyridine)₂]

: 1221191-19-0
2-(dicyclohexylphosphanyl)-N-(2-(dicyclohexylphosphanyl)ethyl)-N-methylethan-1-amine

: [(bis[(2-dicyclohexylphosphino)ethyl]methylamine)cobalt(II)(CH₂SiMe₃)]B(3,5-(CF₃)₂C₆H₃)₄

Guidance literature:: [Co(CH₂SiMe₃)₂(pyridine)₂]; 2-(dicyclohexylphosphanyl)-N-(2-(dicyclohexylphosphanyl)ethyl)-N-methylethan-1-amine; In toluene; at -25 - 20 ℃; for 0.5h; Inert atmosphere;

tetrakis[3,5-bis(trifluoromethyl)phenyl]boric acid bis(diethyl ether) complex; In diethyl ether; for 0.0833333h; Inert atmosphere;
DOI:10.1021/ja402679a