tetraethylammonium diphenyldithiophosphinate

Base Information

Chemical Name:tetraethylammonium diphenyldithiophosphinate
CAS No.:146576-10-5
Molecular Formula:C₈H₂₀N*C₁₂H₁₀PS₂
Molecular Weight:379.571
Hs Code.:

Synonyms:tetraethylammonium diphenyldithiophosphinate

Suppliers and Price of tetraethylammonium diphenyldithiophosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetraethylammonium diphenyldithiophosphinate

Chemical Property:

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Technology Process of tetraethylammonium diphenyldithiophosphinate

There total 2 articles about tetraethylammonium diphenyldithiophosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 2512-59-6
bis(diethyldithiophosphinato)zinc

: 27325-75-3
tetraethylammonium stearate

: 146576-10-5
tetraethylammonium diphenyldithiophosphinate

: 77259-18-8
tetraethylammonium bis(diphenyldithiophosphinato-S) (diphenyldithiophosphinato-SS')zincate

: 557-05-1
zinc stearate

Guidance literature:: In acetone; mixt. (Zn(S2PPh2)2) and (NEt4)(OCOC17H35) in acetone refluxed for 24 h; ppt. (zinc stearate) filtered off, soln. allowed to stand at room temp.for 24 h, (NEt4)(Zn(S2PPh2)3) filtered off, mother-liquor evapd. in vacuo - (NEt4)(S2PPh2);
DOI:10.1039/DT9830000627

Reference yield:

: 1015-38-9
diphenylphosphinodithioic acid

: 146576-10-5
tetraethylammonium diphenyldithiophosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: water; methanol

2: acetone

In methanol; water; acetone;
DOI:10.1039/DT9830000627

Reference yield: 80.0%

: 146576-10-5
tetraethylammonium diphenyldithiophosphinate

: 10139-47-6
zinc(II) iodide

: (NEt₄)(ZnI₂(S₂PPh₂))

Guidance literature:: In acetone; to soln. ZnI2 in acetone added to hot soln. (NEt)(S2PPh2) in acetone, mixt. stirred and heated for 15 min; solvent evapd. in vacuo, oil dissolved in mixt. acetone and propan-2-ol(1:1 v/v), crystals filtered off and washed with acetone; elem. anal.;
DOI:10.1039/DT9830000627