C₂₇H₃₅ClN₈O₄S*ClH

Base Information

Chemical Name:C₂₇H₃₅ClN₈O₄S*ClH
CAS No.:1353624-77-7
Molecular Formula:C₂₇H₃₅ClN₈O₄S*ClH
Molecular Weight:639.606
Hs Code.:

C<sub>27</sub>H<sub>35</sub>ClN<sub>8</sub>O<sub>4</sub>S*ClH

Synonyms:C₂₇H₃₅ClN₈O₄S*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₅ClN₈O₄S*ClH

Chemical Property:

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Technology Process of C₂₇H₃₅ClN₈O₄S*ClH

There total 7 articles about C₂₇H₃₅ClN₈O₄S*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 217806-26-3
tert-butyl N-(azetidin-3-yl)carbamate hydrochloride

: 1353629-21-6
C₂₄H₂₈Cl₂N₆O₄S

: 1353624-77-7
C₂₇H₃₅ClN₈O₄S*ClH

Guidance literature:: tert-butyl N-(azetidin-3-yl)carbamate hydrochloride; C₂₄H₂₈Cl₂N₆O₄S; With triethylamine; In methanol; at 20 - 70 ℃; for 2h;

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 4.5h;

Reference yield:

: 1353629-12-5
C₁₇H₂₂N₄O₂

: 1353624-77-7
C₂₇H₃₅ClN₈O₄S*ClH

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium ethanolate / ethanol / 1 h / 20 - 70 °C / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 1.5 h / 20 °C / Inert atmosphere

3.1: trichlorophosphate / 5 h / 20 - 100 °C

4.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: sodium hydrogencarbonate / acetonitrile; water / 1 h / 20 °C

6.1: triethylamine / methanol / 2 h / 20 - 70 °C

6.2: 4.5 h / 20 °C

With hydrogen; sodium ethanolate; sodium hydrogencarbonate; triethylamine; trichlorophosphate; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 1353631-62-5
(25,5S)-1-benzyl 2-methyl 5-methylpiperidine-1,2-dicarboxylate

: 1353624-77-7
C₂₇H₃₅ClN₈O₄S*ClH

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 1 h

2.1: sodium ethanolate / ethanol / 1 h / 20 - 70 °C / Inert atmosphere

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 1.5 h / 20 °C / Inert atmosphere

4.1: trichlorophosphate / 5 h / 20 - 100 °C

5.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

6.1: sodium hydrogencarbonate / acetonitrile; water / 1 h / 20 °C

7.1: triethylamine / methanol / 2 h / 20 - 70 °C

7.2: 4.5 h / 20 °C

With n-butyllithium; hydrogen; sodium ethanolate; sodium hydrogencarbonate; triethylamine; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile;