Technology Process of C32H41N5O5S
There total 3 articles about C32H41N5O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C36H49N5O5S;
With
trifluoroacetic acid;
for 16h;
With
potassium hydroxide;
In
methanol;
pH=13;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h
1.2: 16 h
2.1: trifluoroacetic acid / 16 h
2.2: pH 13
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1H-imidazole / dichloromethane / 1.5 h
1.2: 16 h
2.1: sodium hydroxide; water / methanol / 3 h / pH 13 - 14
2.2: pH 9
3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h
3.2: 16 h
4.1: trifluoroacetic acid / 16 h
4.2: pH 13
With
1H-imidazole; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; sodium hydroxide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;