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di-adamantan-1-yl-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-phosphane

Base Information Edit
  • Chemical Name:di-adamantan-1-yl-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-phosphane
  • CAS No.:554432-03-0
  • Molecular Formula:C32H49OPSi
  • Molecular Weight:508.8
  • Hs Code.:
  • Mol file:554432-03-0.mol
di-adamantan-1-yl-[4-(<i>tert</i>-butyl-dimethyl-silanyloxy)-phenyl]-phosphane

Synonyms:di-adamantan-1-yl-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-phosphane

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Chemical Property of di-adamantan-1-yl-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-phosphane Edit
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Technology Process of di-adamantan-1-yl-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-phosphane

There total 4 articles about di-adamantan-1-yl-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
t-butyldimethylsilyl-4-bromophenol; With magnesium; In tetrahydrofuran;
With copper(I) bromide; In tetrahydrofuran; at 20 ℃; for 0.333333h;
di-1-adamantylchlorophosphane; In tetrahydrofuran; for 14h; Further stages.; Heating;
DOI:10.1002/chem.200390161
Guidance literature:
Multi-step reaction with 2 steps
1.1: 98 percent / Et3N / CH2Cl2 / 12 h / 20 °C
2.1: Mg / tetrahydrofuran
2.2: CuBr / tetrahydrofuran / 0.33 h / 20 °C
2.3: 63 percent / tetrahydrofuran / 14 h / Heating
With magnesium; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.200390161
Guidance literature:
Multi-step reaction with 2 steps
1.1: 100 percent / CCl4 / 16 h / 50 °C
2.1: Mg / tetrahydrofuran
2.2: CuBr / tetrahydrofuran / 0.33 h / 20 °C
2.3: 63 percent / tetrahydrofuran / 14 h / Heating
With tetrachloromethane; magnesium; In tetrahydrofuran;
DOI:10.1002/chem.200390161
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