5-(4-(9-butyl-9H-pyreno[4,5-d]imidazol-10-yl)phenyl)thiophene-2-carbaldehyde

Base Information

Chemical Name:5-(4-(9-butyl-9H-pyreno[4,5-d]imidazol-10-yl)phenyl)thiophene-2-carbaldehyde
CAS No.:1300113-91-0
Molecular Formula:C₃₂H₂₄N₂OS
Molecular Weight:484.621
Hs Code.:

Synonyms:5-(4-(9-butyl-9H-pyreno[4,5-d]imidazol-10-yl)phenyl)thiophene-2-carbaldehyde

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Chemical Property of 5-(4-(9-butyl-9H-pyreno[4,5-d]imidazol-10-yl)phenyl)thiophene-2-carbaldehyde

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Technology Process of 5-(4-(9-butyl-9H-pyreno[4,5-d]imidazol-10-yl)phenyl)thiophene-2-carbaldehyde

There total 4 articles about 5-(4-(9-butyl-9H-pyreno[4,5-d]imidazol-10-yl)phenyl)thiophene-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1300113-88-5
10-(4-bromophenyl)-9-butyl-9H-pyreno[4,5-d]imidazole

: 349616-56-4
5-(1,3-dioxolan-2-yl)-2-(tributylstannyl)thiophene

: 1300113-91-0
5-(4-(9-butyl-9H-pyreno[4,5-d]imidazol-10-yl)phenyl)thiophene-2-carbaldehyde

Guidance literature:: 10-(4-bromophenyl)-9-butyl-9H-pyreno[4,5-d]imidazole; 5-(1,3-dioxolan-2-yl)-2-(tributylstannyl)thiophene; With bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; at 80 ℃; for 24h; Inert atmosphere;

With acetic acid; In water; at 50 ℃; for 1h;
DOI:10.1021/ol2006874

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1300113-91-0
5-(4-(9-butyl-9H-pyreno[4,5-d]imidazol-10-yl)phenyl)thiophene-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium acetate; acetic acid / 24 h / Reflux

2.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water; benzene / 6 h / Reflux

3.1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere

3.2: 1 h / 50 °C

With bis-triphenylphosphine-palladium(II) chloride; ammonium acetate; N-benzyl-N,N,N-triethylammonium chloride; acetic acid; sodium hydroxide; In water; N,N-dimethyl-formamide; benzene; 3.1: Stille coupling;
DOI:10.1021/ol2006874

Reference yield:

: 6217-22-7
pyrene-4,5-dione

: 1300113-91-0
5-(4-(9-butyl-9H-pyreno[4,5-d]imidazol-10-yl)phenyl)thiophene-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium acetate; acetic acid / 24 h / Reflux

2.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water; benzene / 6 h / Reflux

3.1: bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere

3.2: 1 h / 50 °C

With bis-triphenylphosphine-palladium(II) chloride; ammonium acetate; N-benzyl-N,N,N-triethylammonium chloride; acetic acid; sodium hydroxide; In water; N,N-dimethyl-formamide; benzene; 3.1: Stille coupling;
DOI:10.1021/ol2006874