Technology Process of C22H22FN7O
There total 8 articles about C22H22FN7O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
dimethyl sulfoxide;
for 0.833333h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / acetone / 19 h / 20 °C
2: ammonium acetate / acetic acid / 3 h / 160 °C / Sealed tube
3: trichlorophosphate / 0.33 h / 80 °C
4: N-ethyl-N,N-diisopropylamine; 1-butyl-3-methylimidazolium Tetrafluoroborate / 1-methyl-pyrrolidin-2-one / 2.08 h / 110 °C
5: hydrogenchloride / 1,4-dioxane / 0.5 h / 50 °C
6: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / dimethyl sulfoxide / 0.83 h
With
hydrogenchloride; ammonium acetate; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 1-butyl-3-methylimidazolium Tetrafluoroborate; trichlorophosphate;
In
1,4-dioxane; 1-methyl-pyrrolidin-2-one; acetic acid; dimethyl sulfoxide; acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trichlorophosphate / 0.33 h / 80 °C
2: N-ethyl-N,N-diisopropylamine; 1-butyl-3-methylimidazolium Tetrafluoroborate / 1-methyl-pyrrolidin-2-one / 2.08 h / 110 °C
3: hydrogenchloride / 1,4-dioxane / 0.5 h / 50 °C
4: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; triethylamine / dimethyl sulfoxide / 0.83 h
With
hydrogenchloride; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; 1-butyl-3-methylimidazolium Tetrafluoroborate; trichlorophosphate;
In
1,4-dioxane; 1-methyl-pyrrolidin-2-one; dimethyl sulfoxide;