6-(n-octyl)-9-(C₆H₅-(CH₂)3)-B₁₀H₁₂

Base Information

Chemical Name:6-(n-octyl)-9-(C₆H₅-(CH₂)3)-B₁₀H₁₂
CAS No.:213844-01-0
Molecular Formula:C₁₇H₄₀B₁₀
Molecular Weight:352.615
Hs Code.:

6-(n-octyl)-9-(C<sub>6</sub>H<sub>5</sub>-(CH<sub>2</sub>)3)-B<sub>10</sub>H<sub>12</sub>

Synonyms:6-(n-octyl)-9-(C₆H₅-(CH₂)3)-B₁₀H₁₂

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Chemical Property of 6-(n-octyl)-9-(C₆H₅-(CH₂)3)-B₁₀H₁₂

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Technology Process of 6-(n-octyl)-9-(C₆H₅-(CH₂)3)-B₁₀H₁₂

There total 2 articles about 6-(n-octyl)-9-(C₆H₅-(CH₂)3)-B₁₀H₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 300-57-2,57807-91-7
allylbenzene

: 149002-04-0
6-(n-octyl)decaborane

: 213844-01-0
6-(n-octyl)-9-(C₆H₅-(CH₂)3)-B₁₀H₁₂

Guidance literature:: platinum(II) bromde; In neat (no solvent); under inert atm.; mixt. of PtBr2, 6-(n-octyl)decaborane and allylbenzenein a flask was cooled to -196°C, flask was evacuated, sealed, an d brought to 25°C, heated at 60°C for 4 h; cooled to room temp., soln. exposed to air, mixt. eluted down a silica gel column with benzene/hexanes (1:1), volatiles removed in vac. and thenon the high-vac. line overnight; elem. anal.;
DOI:10.1021/ja011432s

Reference yield: 83.0%

: 300-57-2,57807-91-7
allylbenzene

: 17702-41-9
nido-decaborane

: 149002-04-0
6-(n-octyl)decaborane

: 390745-26-3
6,9-(C₆H₅CH₂CH₂CH₂)2decaborane

: 213844-01-0
6-(n-octyl)-9-(C₆H₅-(CH₂)3)-B₁₀H₁₂

Guidance literature:: dihydrogen hexachloroplatinate(IV) hexahydrate; In neat (no solvent); under inert atm.; a tube with H2PtCl6*6H2O, allylbenzene, decaborane (asinitiator) and 6-(n-octyl)decaborane were cooled to -196°C and e vacuated on a high-vac. line, mixt. warmed to 25°C, heated at 65°C under stirring for 14 h; flash filtering through a silica gel column;
DOI:10.1021/ja011432s