2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Base Information

• Chemical Name: 2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate
• CAS No.: 1031364-37-0
• Molecular Formula: C₃₁H₃₃NO₈
• Molecular Weight: 547.605

Synonyms:2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Chemical Property of 2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Chemical Property:

Purity/Quality:

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Technology Process of 2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

There total 3 articles about 2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-acetoxy-4-methoxycarbonyl-2,6-dimethylbenzene (1031363-89-9) → 2'-(CH2O[CH2CH2O]CH2CH2OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate (1031364-37-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 6 h / Reflux; Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C / Inert atmosphere

2.2: 0.5 h / 0 °C

3.1: pyridine / 0 - 20 °C / Inert atmosphere

3.2: Inert atmosphere

With pyridine; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrahydrofuran; tetrachloromethane; mineral oil;

Reference yield:

methyl 4-hydroxy-3,5-dimethylbenzoate (34137-14-9) → 2'-(CH2O[CH2CH2O]CH2CH2OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate (1031364-37-0)

Guidance literature:

Multi-step reaction with 4 steps

1.1: pyridine / 0 - 20 °C / Inert atmosphere

2.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 6 h / Reflux; Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C / Inert atmosphere

3.2: 0.5 h / 0 °C

4.1: pyridine / 0 - 20 °C / Inert atmosphere

4.2: Inert atmosphere

With pyridine; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrahydrofuran; tetrachloromethane; mineral oil;

Reference yield:

3,5-dimethyl-4-hydroxybenzoic acid (4919-37-3) → 2'-(CH2O[CH2CH2O]CH2CH2OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate (1031364-37-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: thionyl chloride / 20 °C / Cooling with ice

2.1: pyridine / 0 - 20 °C / Inert atmosphere

3.1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 6 h / Reflux; Inert atmosphere

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C / Inert atmosphere

4.2: 0.5 h / 0 °C

5.1: pyridine / 0 - 20 °C / Inert atmosphere

5.2: Inert atmosphere

With pyridine; N-Bromosuccinimide; thionyl chloride; 2,2'-azobis(isobutyronitrile); sodium hydride; In tetrahydrofuran; tetrachloromethane; mineral oil;

upstream raw materials:

methyl 4-hydroxy-3,5-dimethylbenzoate

3,5-dimethyl-4-hydroxybenzoic acid

1-acetoxy-4-methoxycarbonyl-2,6-dimethylbenzene

Downstream raw materials:

C₃₄H₃₉NO₁₁S

NSP-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE

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