benzyl 3,5,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-β-D-glucofuranoside

Base Information

Chemical Name:benzyl 3,5,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-β-D-glucofuranoside
CAS No.:144261-04-1
Molecular Formula:C₆₁H₆₄O₁₁
Molecular Weight:973.173
Hs Code.:

Synonyms:benzyl 3,5,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-β-D-glucofuranoside

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Chemical Property of benzyl 3,5,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-β-D-glucofuranoside

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Technology Process of benzyl 3,5,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-β-D-glucofuranoside

There total 7 articles about benzyl 3,5,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-β-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 144261-03-0
Acetic acid (2R,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-[(2R,3R,4S,5R)-2,4-bis-benzyloxy-5-((R)-1,2-bis-benzyloxy-ethyl)-tetrahydro-furan-3-yloxy]-tetrahydro-pyran-2-ylmethyl ester

: 144261-04-1
benzyl 3,5,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-β-D-glucofuranoside

Guidance literature:: With sodium methylate; In methanol; chloroform;
DOI:10.1016/S0008-6215(00)90992-3

Reference yield:

: 4356-77-8,35094-65-6,61277-56-3,65556-30-1,78185-13-4,78185-15-6,109958-31-8,109958-33-0,113532-02-8,59433-13-5
1,6-di-O-acetyl-2,3,4-tri-O-benzyl-D-glucopyranose

: 144261-04-1
benzyl 3,5,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: TiBr₄ / CH₂Cl₂; ethyl acetate / 1.25 h / Ambient temperature

2: 1) Hg(CN)2, molecular sieves (4 Angstroem) / 1) nitromethane, toluene, 1 h, 2) toluene, r. t., 20 h

3: 94 percent / NaOCH₃ / CHCl₃; methanol

With 4 A molecular sieve; sodium methylate; mercury(II) cyanide; titanium(IV) bromide; In methanol; dichloromethane; chloroform; ethyl acetate;
DOI:10.1016/S0008-6215(00)90992-3

Reference yield:

: 35094-58-7
6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl bromide

: 144261-04-1
benzyl 3,5,6-tri-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Hg(CN)2, molecular sieves (4 Angstroem) / 1) nitromethane, toluene, 1 h, 2) toluene, r. t., 20 h

2: 94 percent / NaOCH₃ / CHCl₃; methanol

With 4 A molecular sieve; sodium methylate; mercury(II) cyanide; In methanol; chloroform;
DOI:10.1016/S0008-6215(00)90992-3