(4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-3-O-methyl-4-phthalimido-α-L-threo-pentopyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trifluoromethanesulfonyl)-β-D-galactopyranoside

Base Information

• Chemical Name: (4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-3-O-methyl-4-phthalimido-α-L-threo-pentopyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trifluoromethanesulfonyl)-β-D-galactopyranoside
• CAS No.: 134262-80-9
• Molecular Formula: C₃₇H₄₀F₃NO₁₃S
• Molecular Weight: 795.785

Synonyms:(4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-3-O-methyl-4-phthalimido-α-L-threo-pentopyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trifluoromethanesulfonyl)-β-D-galactopyranoside

Chemical Property of (4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-3-O-methyl-4-phthalimido-α-L-threo-pentopyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trifluoromethanesulfonyl)-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-3-O-methyl-4-phthalimido-α-L-threo-pentopyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trifluoromethanesulfonyl)-β-D-galactopyranoside

There total 11 articles about (4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-3-O-methyl-4-phthalimido-α-L-threo-pentopyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trifluoromethanesulfonyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,5-anhydro-2,4-dideoxy-3-O-methyl-4-phthalimido-L-threo-pent-1-enopyranose (134262-63-8) → (4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-3-O-methyl-4-phthalimido-α-L-threo-pentopyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trifluoromethanesulfonyl)-β-D-galactopyranoside (134262-80-9)

Guidance literature:

Multi-step reaction with 3 steps

1: I⁽¹⁺⁾*ClO₄^(1-)-(sym-collidine)2 / CH₂Cl₂

2: Ph₃SnH, AIBN / benzene / Heating

3: pyridine

With pyridine; 2,2'-azobis(isobutyronitrile); iodonium(di-γ-collidine) perchlorate; triphenylstannane; In dichloromethane; benzene;

DOI:10.1021/jo951560x

Reference yield:

(4-methoxyphenyl)methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside (134262-79-6) → (4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-3-O-methyl-4-phthalimido-α-L-threo-pentopyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trifluoromethanesulfonyl)-β-D-galactopyranoside (134262-80-9)

Guidance literature:

Multi-step reaction with 3 steps

1: I⁽¹⁺⁾*ClO₄^(1-)-(sym-collidine)2 / CH₂Cl₂

2: Ph₃SnH, AIBN / benzene / Heating

3: pyridine

With pyridine; 2,2'-azobis(isobutyronitrile); iodonium(di-γ-collidine) perchlorate; triphenylstannane; In dichloromethane; benzene;

DOI:10.1021/jo951560x

Reference yield:

(4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside (134262-90-1) → (4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-3-O-methyl-4-phthalimido-α-L-threo-pentopyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-4-O-(trifluoromethanesulfonyl)-β-D-galactopyranoside (134262-80-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Ph₃SnH, AIBN / benzene / Heating

2: pyridine

With pyridine; 2,2'-azobis(isobutyronitrile); triphenylstannane; In benzene;

DOI:10.1021/jo951560x

upstream raw materials:

1,5-anhydro-2,4-dideoxy-3-O-methyl-4-phthalimido-L-threo-pent-1-enopyranose

phenyl 2,4-dideoxy-3-O-methyl-4-phthalimido-1-thio-L-threo-pentopyranoside

(4-methoxyphenyl)methyl 2-O-(2,4-dideoxy-2-iodo-3-O-methyl-4-phthalimido-α-L-lyxo-pyranosyl)-(1<*>2)-6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside

methyl 6-deoxy-3-O-<(4-methoxyphenyl)methyl>-β-D-galactopyranoside

Downstream raw materials:

(4-methoxyphenyl)methyl 4,6-dideoxy-4-<<2,4,6-trideoxy-3-O-<(1,1-dimethylethyl)dimethylsilyl>-4-(methylthio-β-D-ribo-hexopyranosyl)oxy><2-(trimethylsilyl)ethoxycarbonyl>amino>-2-O-(4-amino-2,4-dideoxy-3-O-methyl-α-L-threo-pentopyranosyl)-3-O-...

(4-methoxyphenyl)methyl 4,6-dideoxy-4-<<2,4,6-trideoxy-3-O-<(1,1-dimethylethyl)dimethylsilyl>-4-(methylthio-β-D-ribo-hexopyranosyl)oxy><2-(trimethylsilyl)ethoxycarbonyl>amino>-2-O-<2,4-dideoxy-3-O-methyl-4-<(1-methylethyl)amino>-α-L-threo-pentopyra>..

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