Technology Process of C27H42Br2N6O7
There total 8 articles about C27H42Br2N6O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 79 percent / sodium acetate / acetic anhydride / 3 h / 150 °C / Heating
2: 78 percent / HCl / tetrahydrofuran; H2O / 12 h / 70 °C
3: 76 percent / NH2OH*HCl; NaHCO3 / dioxane / 4 h / 25 - 30 °C
4: 89 percent / NaN3 / dimethylsulfoxide / 8 h / 50 °C
5: 78 percent / N-hydroxyphthalimide; DCC / dioxane / 6 h / 25 - 30 °C
6: 84 percent / Ph3P / tetrahydrofuran; H2O / 24 h / 40 °C
With
hydrogenchloride; sodium azide; N-hydroxyphthalimide; hydroxylamine hydrochloride; sodium acetate; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; water; acetic anhydride; dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2005.07.109
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 76 percent / NH2OH*HCl; NaHCO3 / dioxane / 4 h / 25 - 30 °C
2: 89 percent / NaN3 / dimethylsulfoxide / 8 h / 50 °C
3: 78 percent / N-hydroxyphthalimide; DCC / dioxane / 6 h / 25 - 30 °C
4: 84 percent / Ph3P / tetrahydrofuran; H2O / 24 h / 40 °C
With
sodium azide; N-hydroxyphthalimide; hydroxylamine hydrochloride; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2005.07.109
