1-{3-[(triphenyl-λ⁵-phosphanylidene)amino]pyrazin-2-yl}piperidin-4amine

Base Information

Chemical Name:1-{3-[(triphenyl-λ⁵-phosphanylidene)amino]pyrazin-2-yl}piperidin-4amine
CAS No.:1400820-12-3
Molecular Formula:C₂₇H₂₈N₅P
Molecular Weight:453.527
Hs Code.:

1-{3-[(triphenyl-λ<sup>5</sup>-phosphanylidene)amino]pyrazin-2-yl}piperidin-4amine

Synonyms:1-{3-[(triphenyl-λ⁵-phosphanylidene)amino]pyrazin-2-yl}piperidin-4amine

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Chemical Property of 1-{3-[(triphenyl-λ⁵-phosphanylidene)amino]pyrazin-2-yl}piperidin-4amine

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Technology Process of 1-{3-[(triphenyl-λ⁵-phosphanylidene)amino]pyrazin-2-yl}piperidin-4amine

There total 2 articles about 1-{3-[(triphenyl-λ⁵-phosphanylidene)amino]pyrazin-2-yl}piperidin-4amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1400820-50-9
tert-butyl(1-{3-[(triphenyl-λ⁵-phosphanylidene)amino]pyrazin-2-yl}piperidin-4-yl)carbamate

: 1400820-12-3
1-{3-[(triphenyl-λ⁵-phosphanylidene)amino]pyrazin-2-yl}piperidin-4amine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 0.166667h;
DOI:10.1016/j.tetlet.2012.07.106

Reference yield:

: 1400820-08-7
(chloropyrazin-2-yl)imino-triphenyl-λ⁵-phosphane

: 1400820-12-3
1-{3-[(triphenyl-λ⁵-phosphanylidene)amino]pyrazin-2-yl}piperidin-4amine

Guidance literature:: Multi-step reaction with 2 steps

1: 1-methyl-pyrrolidin-2-one / 130 °C

2: trifluoroacetic acid / dichloromethane / 0.17 h / 0 - 20 °C

With trifluoroacetic acid; In 1-methyl-pyrrolidin-2-one; dichloromethane;
DOI:10.1016/j.tetlet.2012.07.106