(R,R)-N¹-[(2-benzoylamino-adamantan-2-yl)carbonyl]-1,2-diphenylethylenediamine

Base Information

Chemical Name:(R,R)-N¹-[(2-benzoylamino-adamantan-2-yl)carbonyl]-1,2-diphenylethylenediamine
CAS No.:1374765-39-5
Molecular Formula:C₃₂H₃₅N₃O₂
Molecular Weight:493.649
Hs Code.:

(R,R)-N<sup>1</sup>-[(2-benzoylamino-adamantan-2-yl)carbonyl]-1,2-diphenylethylenediamine

Synonyms:(R,R)-N¹-[(2-benzoylamino-adamantan-2-yl)carbonyl]-1,2-diphenylethylenediamine

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Chemical Property of (R,R)-N¹-[(2-benzoylamino-adamantan-2-yl)carbonyl]-1,2-diphenylethylenediamine

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Technology Process of (R,R)-N¹-[(2-benzoylamino-adamantan-2-yl)carbonyl]-1,2-diphenylethylenediamine

There total 4 articles about (R,R)-N¹-[(2-benzoylamino-adamantan-2-yl)carbonyl]-1,2-diphenylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1374765-29-3
2-phenyl-4-(adamantane-2'-spiro)-oxazolin-5-one

: 35132-20-8
(R,R)-1,2-diphenylethylenediamine

: 1374765-39-5
(R,R)-N¹-[(2-benzoylamino-adamantan-2-yl)carbonyl]-1,2-diphenylethylenediamine

Guidance literature:: In tetrahydrofuran; at 60 ℃; for 0.116667h;
DOI:10.1021/op300084z

Reference yield:

: 1374765-28-2
2-phenyl-4-(adamantane-2'-spiro)-5-methylidene-oxazoline

: 1374765-39-5
(R,R)-N¹-[(2-benzoylamino-adamantan-2-yl)carbonyl]-1,2-diphenylethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: ozone / dichloromethane / 0 h / 375.04 Torr

2: tetrahydrofuran / 0.12 h / 60 °C

With ozone; In tetrahydrofuran; dichloromethane;
DOI:10.1021/op300084z

Reference yield:

: 700-58-3
2-Adamantanone

: 1374765-39-5
(R,R)-N¹-[(2-benzoylamino-adamantan-2-yl)carbonyl]-1,2-diphenylethylenediamine

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 0.62 h / 40 °C

2: sulfuric acid / acetic anhydride; acetic acid / 0.19 h / 30 °C

3: potassium hydroxide / ethanol / 0.4 h / 120 °C / 5171.62 Torr

4: ozone / dichloromethane / 0 h / 375.04 Torr

5: tetrahydrofuran / 0.12 h / 60 °C

With sulfuric acid; ozone; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; acetic anhydride; acetic acid; 1: Grignard reaction / 2: Ritter reaction;
DOI:10.1021/op300084z