2-[(6-(4-chlorophenyl)-3-cyano-4-(2-nitrophenyl)pyridin-2-yl)sulfanyl]-1-phenylethylidenemalononitrile

Base Information

Chemical Name:2-[(6-(4-chlorophenyl)-3-cyano-4-(2-nitrophenyl)pyridin-2-yl)sulfanyl]-1-phenylethylidenemalononitrile
CAS No.:1416454-01-7
Molecular Formula:C₂₉H₁₆ClN₅O₂S
Molecular Weight:533.997
Hs Code.:

Synonyms:2-[(6-(4-chlorophenyl)-3-cyano-4-(2-nitrophenyl)pyridin-2-yl)sulfanyl]-1-phenylethylidenemalononitrile

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Chemical Property of 2-[(6-(4-chlorophenyl)-3-cyano-4-(2-nitrophenyl)pyridin-2-yl)sulfanyl]-1-phenylethylidenemalononitrile

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Technology Process of 2-[(6-(4-chlorophenyl)-3-cyano-4-(2-nitrophenyl)pyridin-2-yl)sulfanyl]-1-phenylethylidenemalononitrile

There total 4 articles about 2-[(6-(4-chlorophenyl)-3-cyano-4-(2-nitrophenyl)pyridin-2-yl)sulfanyl]-1-phenylethylidenemalononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1416453-92-3
6-(4-chlorophenyl)-4-(2-nitrophenyl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile

: 4651-78-9
2-bromo-1-phenylethylidenemalononitrile

: 1416454-01-7
2-[(6-(4-chlorophenyl)-3-cyano-4-(2-nitrophenyl)pyridin-2-yl)sulfanyl]-1-phenylethylidenemalononitrile

Guidance literature:: With piperidine; In ethanol; at 50 ℃; for 12h;
DOI:10.1007/s12272-012-1107-6

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 1416454-01-7
2-[(6-(4-chlorophenyl)-3-cyano-4-(2-nitrophenyl)pyridin-2-yl)sulfanyl]-1-phenylethylidenemalononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / butan-1-ol / 9 h / Reflux

2: piperidine / ethanol / 12 h / 50 °C

With piperidine; ammonium acetate; In ethanol; butan-1-ol;
DOI:10.1007/s12272-012-1107-6

Reference yield:

: 24668-08-4
1-(4-chlorophenyl)-3-(2-nitrophenyl)prop-2-en-1-one

: 1416454-01-7
2-[(6-(4-chlorophenyl)-3-cyano-4-(2-nitrophenyl)pyridin-2-yl)sulfanyl]-1-phenylethylidenemalononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: sodium ethanolate / ethanol / 7 h / Reflux

2: piperidine / ethanol / 12 h / 50 °C

With piperidine; sodium ethanolate; In ethanol;
DOI:10.1007/s12272-012-1107-6