4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepan-1-ium Trifluoroacetate

Base Information

Chemical Name:4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepan-1-ium Trifluoroacetate
CAS No.:959841-46-4
Molecular Formula:C₂HF₃O₂*C₁₉H₂₂ClFN₄O
Molecular Weight:490.885
Hs Code.:

Synonyms:4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepan-1-ium Trifluoroacetate

Suppliers and Price of 4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepan-1-ium Trifluoroacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepan-1-ium Trifluoroacetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepan-1-ium Trifluoroacetate

There total 4 articles about 4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepan-1-ium Trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 959841-44-2
5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoic Acid

: 112275-50-0
tert-butyl 1,4-diazepine-1-carboxylate

: 959841-46-4
4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepan-1-ium Trifluoroacetate

Guidance literature:: With hydrogenchloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In ethanol; water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; 2,4-dichlorophenoxyacetic acid dimethylamine; acetonitrile;

Reference yield:

: 959841-45-3
4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepane

: 76-05-1
trifluoroacetic acid

: 959841-46-4
4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepan-1-ium Trifluoroacetate

Guidance literature:: In water; acetonitrile;

Reference yield:

: 959841-42-0
5-[(6-chloro-4-ethylpyridazin-3-yl)(cyano)methyl]-2-fluorobenzonitrile

: 959841-46-4
4-{5-[(6-chloro-4-ethylpyridazin-3-yl)methyl]-2-fluorobenzoyl}-1,4-diazepan-1-ium Trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; water; acetic acid / acetic acid / Heating / reflux

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 20 °C

3.1: hydrogenchloride; ethanol / 2 h / 20 °C

3.2: pH 9

4.1: water; acetonitrile

With hydrogenchloride; ethanol; water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl acetamide; water; acetic acid; acetonitrile;