C₁₁H₉F₃O₂

Base Information

Chemical Name:C₁₁H₉F₃O₂
CAS No.:1312756-43-6
Molecular Formula:C₁₁H₉F₃O₂
Molecular Weight:230.186
Hs Code.:

C<sub>11</sub>H<sub>9</sub>F<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₁H₉F₃O₂

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Chemical Property of C₁₁H₉F₃O₂

Chemical Property:

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Technology Process of C₁₁H₉F₃O₂

There total 3 articles about C₁₁H₉F₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1080636-43-6
3-[4-(trifluoromethyl)phenyl]cyclobutanone

: 1312756-43-6
C₁₁H₉F₃O₂

: C₁₁H₉F₃O₂

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); silver hexafluoroantimonate; urea hydrogen peroxide adduct; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; In tetrahydrofuran; at -40 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1016/j.tet.2011.04.046

Reference yield:

: 2,2-dichloro-3-[4-(trifluoromethyl)phenyl]cyclobutanone

: 1312756-43-6
C₁₁H₉F₃O₂

: C₁₁H₉F₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium chloride; zinc / methanol / Reflux

2: dichloro bis(acetonitrile) palladium(II); silver hexafluoroantimonate; urea hydrogen peroxide adduct; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / tetrahydrofuran / -40 °C

With dichloro bis(acetonitrile) palladium(II); silver hexafluoroantimonate; urea hydrogen peroxide adduct; ammonium chloride; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; zinc; In tetrahydrofuran; methanol; 2: Baeyer-Villiger oxidation;
DOI:10.1016/j.tet.2011.04.046

Reference yield:

: 402-50-6
1-trifluoromethyl-4-vinyl-benzene

: 1312756-43-6
C₁₁H₉F₃O₂

: C₁₁H₉F₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1: zinc/copper couple; trichlorophosphate / diethyl ether / 40 °C

2: ammonium chloride; zinc / methanol / Reflux

3: dichloro bis(acetonitrile) palladium(II); silver hexafluoroantimonate; urea hydrogen peroxide adduct; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / tetrahydrofuran / -40 °C

With dichloro bis(acetonitrile) palladium(II); silver hexafluoroantimonate; zinc/copper couple; urea hydrogen peroxide adduct; ammonium chloride; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; zinc; trichlorophosphate; In tetrahydrofuran; methanol; diethyl ether; 3: Baeyer-Villiger oxidation;
DOI:10.1016/j.tet.2011.04.046