CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽²⁺⁾*2PF₆^(1-)=(CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)(PF₆)2

Base Information

• Chemical Name: CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽²⁺⁾*2PF₆^(1-)=(CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)(PF₆)2
• CAS No.: 84109-47-7
• Molecular Formula: C₅₂H₅₅FeN₇*2F₆P
• Molecular Weight: 1123.83

Synonyms:CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽²⁺⁾*2PF₆^(1-)=(CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)(PF₆)2

Chemical Property of CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽²⁺⁾*2PF₆^(1-)=(CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)(PF₆)2

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Technology Process of CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽²⁺⁾*2PF₆^(1-)=(CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)(PF₆)2

There total 1 articles about CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽²⁺⁾*2PF₆^(1-)=(CH₃CNC₆H₄(CH₂NCH₂C₆H₅CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)(PF₆)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

Fe(py)2Cl2 (15616-26-9) + H4C6H4(CH2NCH2C6H5CC6H5C3HCH3N2(CH2)3)2(4+)*3PF6(1-)*Cl(1-)=(H4C6H4(CH2NCH2C6H5CC6H5C3HCH3N2(CH2)3)2)(PF6)3Cl → CH3CNC6H4(CH2NCH2C6H5CC6H5C3HCH3N2(CH2)3)2Fe(2+)*2PF6(1-)=(CH3CNC6H4(CH2NCH2C6H5CC6H5C3HCH3N2(CH2)3)2Fe)(PF6)2 (84109-47-7)

Guidance literature:

With triethylamine; acetonitrile; In acetonitrile; ligand and slight excess of Fe complex slurring in MeCN; large excess of Et3N adding, refluxing for 5 min, cooling and filtering through celite, solvent removing, residue dissolving in hot MeOH, stirring for 10 min,filtering; purified by recrystn. from MeCN/EtOH or MeOH; identified by elem. anal.;

DOI:10.1021/ja00360a008

upstream raw materials:

Fe(py)2Cl₂

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