Technology Process of C35H42O8
There total 11 articles about C35H42O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C30H33IO8;
With
Zn(iPr)2; [Li(acac)];
In
1-methyl-pyrrolidin-2-one;
prenyl bromide;
With
CuCN*2LiCl;
Further stages.;
DOI:10.1002/anie.200700895
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 94 percent / Et3N; 4-dimethylaminopyridine / toluene
2.1: 74 percent / Et3N; H2 / [PdCl2(PPh3)2]; CuI / 760.05 Torr
3.1: 84 percent / CO; 4-Angstroem MS / PtCl2 / toluene / 5.5 h / 85 °C / 760.05 Torr
4.1: 82 percent / (NH4)2Ce(NO3)6; CAN / acetonitrile; H2O
5.1: Zn(iPr)2; [Li(acac)] / 1-methyl-pyrrolidin-2-one
5.2: 86 percent / CuCN*2LiCl
With
dmap; ammonium cerium(IV) nitrate; carbon monoxide; 4-Angstroem MS; hydrogen; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; platinum(II) chloride;
In
1-methyl-pyrrolidin-2-one; water; toluene; acetonitrile;
2.1: Sonogashira reaction;
DOI:10.1002/anie.200700895
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 74 percent / Et3N; H2 / [PdCl2(PPh3)2]; CuI / 760.05 Torr
2.1: 84 percent / CO; 4-Angstroem MS / PtCl2 / toluene / 5.5 h / 85 °C / 760.05 Torr
3.1: 82 percent / (NH4)2Ce(NO3)6; CAN / acetonitrile; H2O
4.1: Zn(iPr)2; [Li(acac)] / 1-methyl-pyrrolidin-2-one
4.2: 86 percent / CuCN*2LiCl
With
ammonium cerium(IV) nitrate; carbon monoxide; 4-Angstroem MS; hydrogen; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; platinum(II) chloride;
In
1-methyl-pyrrolidin-2-one; water; toluene; acetonitrile;
1.1: Sonogashira reaction;
DOI:10.1002/anie.200700895
