(2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Base Information

Chemical Name:(2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate
CAS No.:1393727-35-9
Molecular Formula:C₅₀H₃₈O₆S
Molecular Weight:766.914
Hs Code.:

Synonyms:(2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Suppliers and Price of (2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

There total 8 articles about (2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1393727-79-1
(2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-thiobis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

: 1393727-35-9
(2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1016/j.tet.2012.06.001

Reference yield:

: C₂₅H₂₀O₃

: 1393727-35-9
(2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 0.17 h / 0 °C

2: lithium bromide / tetrahydrofuran / 2 h / 20 °C

3: sodium sulfide / methanol / 0.25 h / 20 °C

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 °C

With sodium sulfide; triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium bromide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tet.2012.06.001

Reference yield:

: C₂₆H₂₂O₅S

: 1393727-35-9
(2E,2'E)-dibenzhydryl 3,3'-(2,2'-(3,3'-sulfonylbis(prop-1-yne-3,1-diyl))bis(2,1-phenylene))diacrylate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium bromide / tetrahydrofuran / 2 h / 20 °C

2: sodium sulfide / methanol / 0.25 h / 20 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 °C

With sodium sulfide; 3-chloro-benzenecarboperoxoic acid; lithium bromide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tet.2012.06.001