C₃₁H₄₂N₂O₄*BrH

Base Information

Chemical Name:C₃₁H₄₂N₂O₄*BrH
CAS No.:1561902-56-4
Molecular Formula:BrH*C₃₁H₄₂N₂O₄
Molecular Weight:587.597
Hs Code.:

C<sub>31</sub>H<sub>42</sub>N<sub>2</sub>O<sub>4</sub>*BrH

Synonyms:C₃₁H₄₂N₂O₄*BrH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₄₂N₂O₄*BrH

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Technology Process of C₃₁H₄₂N₂O₄*BrH

There total 7 articles about C₃₁H₄₂N₂O₄*BrH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1561903-45-4
C₃₃H₄₆N₂O₄*ClH

: 1561902-56-4
C₃₁H₄₂N₂O₄*BrH

Guidance literature:: With hydrogen bromide; at 150 ℃; for 2h; Inert atmosphere; Sealed tube; Darkness;
DOI:10.1039/c3ob42309c

Reference yield:

: 947-04-6,25038-74-8
2-azacyclotridecanone

: 1561902-56-4
C₃₁H₄₂N₂O₄*BrH

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere; Reflux

2.1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

4.1: sodium iodide / tetrahydrofuran / 0.42 h / 20 °C / Inert atmosphere

4.2: 1 h / 20 °C

5.1: methanol / 0.5 h

5.2: 16 h / 45 °C

6.1: hydrogenchloride / methanol; diethyl ether; chloroform; pentane

7.1: hydrogen bromide / 2 h / 150 °C / Inert atmosphere; Sealed tube; Darkness

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen bromide; triethylamine; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; chloroform; N,N-dimethyl-formamide; pentane;
DOI:10.1039/c3ob42309c

Reference yield:

: 295-03-4
azacyclotridecane

: 1561902-56-4
C₃₁H₄₂N₂O₄*BrH

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

3.1: sodium iodide / tetrahydrofuran / 0.42 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C

4.1: methanol / 0.5 h

4.2: 16 h / 45 °C

5.1: hydrogenchloride / methanol; diethyl ether; chloroform; pentane

6.1: hydrogen bromide / 2 h / 150 °C / Inert atmosphere; Sealed tube; Darkness

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen bromide; triethylamine; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; chloroform; N,N-dimethyl-formamide; pentane;
DOI:10.1039/c3ob42309c