C₁₅H₉BrFNO₃

Base Information

Chemical Name:C₁₅H₉BrFNO₃
CAS No.:1089178-94-8
Molecular Formula:C₁₅H₉BrFNO₃
Molecular Weight:350.144
Hs Code.:

C<sub>15</sub>H<sub>9</sub>BrFNO<sub>3</sub>

Synonyms:C₁₅H₉BrFNO₃

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Chemical Property of C₁₅H₉BrFNO₃

Chemical Property:

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Technology Process of C₁₅H₉BrFNO₃

There total 7 articles about C₁₅H₉BrFNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1089178-93-7
C₁₇H₁₃BrFNO₄

: 1089178-94-8
C₁₅H₉BrFNO₃

Guidance literature:: With water; toluene-4-sulfonic acid; In acetonitrile; at 20 - 70 ℃;

Reference yield:

: 1089178-86-8
C₁₃H₁₈BrNOSi

: 1089178-94-8
C₁₅H₉BrFNO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran; n-heptane; toluene / 1.83 h / -50 - 20 °C

1.2: -10 - 20 °C

2.1: toluene-4-sulfonic acid / n-heptane; toluene / 100 °C / Heating / reflux

3.1: sodium hydroxide; water / 1,2-dimethoxyethane; toluene / 0.5 h / -20 - 25 °C

3.2: 0 °C / pH 6 - 7

4.1: potassium carbonate / ISOPROPYLAMIDE / 0.08 h

4.2: 0.92 h / 125 °C

5.1: isopropylmagnesium chloride / toluene / 4 h / -78 - -20 °C

5.2: -78 - 20 °C

6.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0 - 20 °C

7.1: water / toluene-4-sulfonic acid / acetonitrile / 20 - 70 °C

With sodium hydroxide; sodium tetrahydroborate; water; isopropylmagnesium chloride; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; n-heptane; ISOPROPYLAMIDE; toluene; acetonitrile;

Reference yield:

: 1089178-88-0
C₁₀H₉NO₃

: 1089178-94-8
C₁₅H₉BrFNO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / ISOPROPYLAMIDE / 0.08 h

1.2: 0.92 h / 125 °C

2.1: isopropylmagnesium chloride / toluene / 4 h / -78 - -20 °C

2.2: -78 - 20 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0 - 20 °C

4.1: water / toluene-4-sulfonic acid / acetonitrile / 20 - 70 °C

With sodium tetrahydroborate; water; isopropylmagnesium chloride; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; ISOPROPYLAMIDE; toluene; acetonitrile;