(2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]-benzoxazole-3-carboxaldehyde

Base Information

Chemical Name:(2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]-benzoxazole-3-carboxaldehyde
CAS No.:244628-35-1
Molecular Formula:C₃₄H₅₃NO₄
Molecular Weight:539.799
Hs Code.:

(2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]-benzoxazole-3-carboxaldehyde

Synonyms:(2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]-benzoxazole-3-carboxaldehyde

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Chemical Property of (2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]-benzoxazole-3-carboxaldehyde

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Technology Process of (2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]-benzoxazole-3-carboxaldehyde

There total 5 articles about (2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]-benzoxazole-3-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 244628-34-0
(2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]benzoxazole-3-carboxylic acid ethyl ester

: 244628-35-1
(2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]-benzoxazole-3-carboxaldehyde

: C₃₄H₅₅NO₄

Guidance literature:: With diisobutylaluminium hydride; In toluene; at -78 ℃; for 1h;
DOI:10.1021/ol990734k

Reference yield:

: C₃₄H₅₅NO₄

: 244628-35-1
(2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]-benzoxazole-3-carboxaldehyde

Guidance literature:: With tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/ol990734k

Reference yield:

: (+)-3-(hydroxylamino)isoborneol hydrochloride

: 244628-35-1
(2S,3S,3aS,4aS,5R,8S,8aR,2'R)-2-(2'-phenylmethyloxy-tridecyl)-5,10,10-trimethyl-5,8-methano-octahydro-2H-isoxazolo-[3,2-b]-benzoxazole-3-carboxaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: calcium carbonate; 4 Angstroem molecular sieves / toluene / 4 h / 40 °C

2: 1.56 g / toluene / 16 h / 80 °C

3: 76 percent / DIBAH / toluene / 1 h / -78 °C

With 4 A molecular sieve; diisobutylaluminium hydride; calcium carbonate; In toluene;
DOI:10.1021/ol990734k