N⁽⁶⁾-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine

Base Information

• Chemical Name: N⁽⁶⁾-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine
• CAS No.: 1040239-15-3
• Molecular Formula: C₄₁H₃₉N₅O₇
• Molecular Weight: 713.79

Synonyms:N⁽⁶⁾-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine

Chemical Property of N⁽⁶⁾-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine

Chemical Property:

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Technology Process of N⁽⁶⁾-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine

There total 1 articles about N⁽⁶⁾-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N(6)-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine (1040239-11-9) → N(6)-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine (1040239-15-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 23 ℃; for 4.25h; Molecular sieve;

DOI:10.1002/hlca.200890071

Reference yield: 77.0%

N(6)-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine (1040239-15-3) + acetic anhydride (108-24-7) → 5'-O-acetyl-N(6)-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine (1040239-21-1)

Guidance literature:

In pyridine; at 24 ℃; for 48h; Inert atmosphere;

DOI:10.1002/hlca.200890071

Reference yield:

N(6)-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine (1040239-15-3) + p-toluenesulfonyl chloride (98-59-9) → C48H45N5O9S

Guidance literature:

With dmap; In dichloromethane; at -10 - 10 ℃; Inert atmosphere;

DOI:10.1002/hlca.200890071

upstream raw materials:

N⁽⁶⁾-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine

Downstream raw materials:

5'-O-acetyl-N⁽⁶⁾-benzoyl-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine

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