2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2,4,6-tri-O-benzoyl-3-O-(prop-3-tert-butyldimethylsilyl-2-yn-1-yl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl azide

Base Information

• Chemical Name: 2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2,4,6-tri-O-benzoyl-3-O-(prop-3-tert-butyldimethylsilyl-2-yn-1-yl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl azide
• CAS No.: 1385067-76-4
• Molecular Formula: C₁₀₆H₁₀₇N₃O₃₂Si
• Molecular Weight: 1963.1

Synonyms:2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2,4,6-tri-O-benzoyl-3-O-(prop-3-tert-butyldimethylsilyl-2-yn-1-yl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl azide

Chemical Property of 2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2,4,6-tri-O-benzoyl-3-O-(prop-3-tert-butyldimethylsilyl-2-yn-1-yl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl azide

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Technology Process of 2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2,4,6-tri-O-benzoyl-3-O-(prop-3-tert-butyldimethylsilyl-2-yn-1-yl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl azide

There total 1 articles about 2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2,4,6-tri-O-benzoyl-3-O-(prop-3-tert-butyldimethylsilyl-2-yn-1-yl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-O-benzoyl-4,6-O-benzylidene-3-O-[4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-{2-Oacetyl-4,6-O-benzylidene-3-O-[2,4,6-tri-O-benzoyl-3-O-(3-tert-butyldimethylsilylprop-2-yn-1-yl)-β-D-glucopyranosyl]-β-D-glucopyranosyl}-β-D-glucopyranosyl)-β-D-glucopyranosyl]-β-D-glucopyranosyl azide (1385068-47-2) + acetic anhydride (108-24-7) → 2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2,4,6-tri-O-benzoyl-3-O-(prop-3-tert-butyldimethylsilyl-2-yn-1-yl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl azide (1385067-76-4)

Guidance literature:

With pyridine; dmap; at 20 ℃; for 2h;

DOI:10.1016/j.tetlet.2012.05.111

Reference yield: 100.0%

2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-(2-O-acetyl-4,6-O-benzylidene-3-O-(2,4,6-tri-O-benzoyl-3-O-(prop-3-tert-butyldimethylsilyl-2-yn-1-yl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl)-β-D-glucopyranosyl azide (1385067-76-4) + N-tert-Butoxycarbonyl-1-amino-3-propyne (92136-39-5) → 1-{2-O-benzoyl-4,6-O-benzylidene-3-O-[2-O-acetyl-4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-{2-O-acetyl-4,6-O-benzylidene-3-O-[2,4,6-tri-O-benzoyl-3-O-(3-tert-butyldimethylsilylprop-2-yn-1-yl)-β-D-glucopyranosyl]-β-D-glucopyranosyl}-β-D-glucopyranosyl)-β-D-glucopyranosyl]-β-D-glucopyranosyl}-4-N-(tert-butoxycarbonyl)aminomethyl-1H-1,2,3-triazole (1385068-52-9)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃; for 48h;

DOI:10.1016/j.tetlet.2012.05.111

upstream raw materials:

2-O-benzoyl-4,6-O-benzylidene-3-O-[4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-{2-Oacetyl-4,6-O-benzylidene-3-O-[2,4,6-tri-O-benzoyl-3-O-(3-tert-butyldimethylsilylprop-2-yn-1-yl)-β-D-glucopyranosyl]-β-D-glucopyranosyl}-β-D-glucopyranosyl)-β-D-glucopyranosyl]-β-D-glucopyranosyl azide

acetic anhydride

Downstream raw materials:

1-{2-O-benzoyl-4,6-O-benzylidene-3-O-[2-O-acetyl-4,6-O-benzylidene-3-O-(2-O-benzoyl-4,6-O-benzylidene-3-O-{2-O-acetyl-4,6-O-benzylidene-3-O-[2,4,6-tri-O-benzoyl-3-O-(3-tert-butyldimethylsilylprop-2-yn-1-yl)-β-D-glucopyranosyl]-β-D-glucopyranosyl}-β-D-glucopyranosyl)-β-D-glucopyranosyl]-β-D-glucopyranosyl}-4-N-(tert-butoxycarbonyl)aminomethyl-1H-1,2,3-triazole

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