4-Anilino-1-methyl-3-nitroquinolin-2(1H)-one

Base Information

Chemical Name:4-Anilino-1-methyl-3-nitroquinolin-2(1H)-one
CAS No.:141945-56-4
Molecular Formula:C16H13 N3 O3
Molecular Weight:295.2927
Hs Code.:
DSSTox Substance ID:DTXSID20383029
Wikidata:Q82174576
Mol file:141945-56-4.mol

Synonyms:DTXSID20383029;4-Anilino-1-methyl-3-nitroquinolin-2(1H)-one;141945-56-4

Suppliers and Price of 4-Anilino-1-methyl-3-nitroquinolin-2(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-Anilino-1-methyl-3-nitroquinolin-2(1H)-one

Chemical Property:

Vapor Pressure:5.76E-07mmHg at 25°C
Boiling Point:411°Cat760mmHg
Flash Point:202.4°C
Density:1.38g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:295.09569129
Heavy Atom Count:22
Complexity:491

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=CC=CC=C2C(=C(C1=O)[N+](=O)[O-])NC3=CC=CC=C3

Technology Process of 4-Anilino-1-methyl-3-nitroquinolin-2(1H)-one

There total 3 articles about 4-Anilino-1-methyl-3-nitroquinolin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 79966-13-5
4-chloro-1-methyl-3-nitro-2-(1H)quinolinone

: 62-53-3
aniline

: 141945-56-4
1-methyl-4-phenylamino-3-nitro-2(1H)-quinolone

Guidance literature:: With triethylamine; In various solvent(s); Ambient temperature;

Reference yield:

: 1677-46-9
4-hydroxy-1-methyl-2(1H)-quinolone

: 141945-56-4
1-methyl-4-phenylamino-3-nitro-2(1H)-quinolone

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / conc. HNO₃, NaNO₂ / acetic acid / 0.5 h

2: 92 percent / triethylamine, phosphoryl chloride / 1 h / Heating

3: 98 percent / Et₃N / various solvent(s) / Ambient temperature

With nitric acid; triethylamine; sodium nitrite; trichlorophosphate; In acetic acid;

Reference yield:

: 36949-55-0
4-hydroxy-1-methyl-3-nitro-2-(1H)quinolinone

: 141945-56-4
1-methyl-4-phenylamino-3-nitro-2(1H)-quinolone

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / triethylamine, phosphoryl chloride / 1 h / Heating

2: 98 percent / Et₃N / various solvent(s) / Ambient temperature

With triethylamine; trichlorophosphate; In various solvent(s);