trans-bis(1H-benzimidazole-κN(3))bis(1H-benzimidazole-2-carboxylato-κ(2)N**(3),O)nickel(II)

Base Information

Chemical Name:trans-bis(1H-benzimidazole-κN**(3))bis(1H-benzimidazole-2-carboxylato-κ**(2)N**(3),O)nickel(II)
CAS No.:1355612-47-3
Molecular Formula:C₃₀H₂₂N₈NiO₄
Molecular Weight:617.246
Hs Code.:

Synonyms:trans-bis(1H-benzimidazole-κN**(3))bis(1H-benzimidazole-2-carboxylato-κ**(2)N**(3),O)nickel(II)

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Chemical Property of trans-bis(1H-benzimidazole-κN**(3))bis(1H-benzimidazole-2-carboxylato-κ**(2)N**(3),O)nickel(II)

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Technology Process of trans-bis(1H-benzimidazole-κN**(3))bis(1H-benzimidazole-2-carboxylato-κ**(2)N**(3),O)nickel(II)

There total 1 articles about trans-bis(1H-benzimidazole-κN**(3))bis(1H-benzimidazole-2-carboxylato-κ**(2)N**(3),O)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 51-17-2,79351-71-6
benzoimidazole

: 2849-93-6
2-benzimidazolecarboxylic acid

: nickel(II) chloride hexahydrate

: 1355612-47-3
trans-bis(1H-benzimidazole-κN**(3))bis(1H-benzimidazole-2-carboxylato-κ**(2)N**(3),O)nickel(II)

Guidance literature:: In ethanol; water; High Pressure; mixt. of NiCl2*6H2O, acid and benzimidazole in H2O/EtOH (3:1 v/v) sealedin sample bottle reactor, heated at 383 K under autogeneous pressure fo r 48 h, cooled to room temp. at 5 K/h;
DOI:10.1107/S0108270111041837