(S)-tert-butyl 2-((S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanamido)propanoate

Base Information

Chemical Name:(S)-tert-butyl 2-((S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanamido)propanoate
CAS No.:124028-06-4
Molecular Formula:C₂₀H₃₀N₂O₅
Molecular Weight:378.469
Hs Code.:

Synonyms:(S)-tert-butyl 2-((S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanamido)propanoate

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Chemical Property of (S)-tert-butyl 2-((S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanamido)propanoate

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Technology Process of (S)-tert-butyl 2-((S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanamido)propanoate

There total 22 articles about (S)-tert-butyl 2-((S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 21691-50-9
Ala-OtBu

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 124028-06-4
(S)-tert-butyl 2-((S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanamido)propanoate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 25 ℃; Inert atmosphere;

Reference yield: 59.0%

: 1432584-72-9
(S,Z)-N-((S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutylidene)-1-(tert-butoxy)-1-oxopropan-2-amine oxide

: 124028-06-4
(S)-tert-butyl 2-((S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanamido)propanoate

: 84765-39-9
(S)-tert-butyl 2-formamidopropanoate

Guidance literature:: In acetonitrile; at 40 ℃; for 1.66667h; Inert atmosphere; UV-irradiation;
DOI:10.1002/anie.201300504

Reference yield:

: 21691-50-9
Ala-OtBu

: C₁₈H₂₅NO₅S

: 124028-06-4
(S)-tert-butyl 2-((S)-2-(((benzyloxy)carbonyl)amino)-3-methylbutanamido)propanoate

Guidance literature:: C₁₈H₂₅NO₅S; With silver tetrafluoroborate; In acetonitrile; at 20 ℃; for 0.0833333h; Inert atmosphere;

Ala-OtBu; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol401053y